4-CH₃C₆H₄BI₂

Base Information

• Chemical Name: 4-CH₃C₆H₄BI₂
• CAS No.: 27545-47-7
• Molecular Formula: C₇H₇BI₂
• Molecular Weight: 355.753
• Mol file: 27545-47-7.mol

Synonyms:4-CH₃C₆H₄BI₂

Chemical Property of 4-CH₃C₆H₄BI₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-CH₃C₆H₄BI₂

There total 11 articles about 4-CH₃C₆H₄BI₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

4-tolyl iodide (624-31-7) + boron triiodide (13517-10-7) → 4-CH3C6H4BI2 (27545-47-7)

Guidance literature:

byproducts: I2; in 30 min at 110°C; I2 sublimated off at 60-70°C/1 Torr; distn.;

DOI:10.1016/S0022-328X(00)87704-9 DOI:10.1016/S0022-328X(00)87829-8

Reference yield:

boron triiodide (13517-10-7) + toluene (108-88-3,15644-74-3,16713-13-6) → 4-CH3C6H4BI2 (27545-47-7) + (3-methylphenyl)diiodoborane (30094-23-6)

Guidance literature:

140°C;

Reference yield:

ortho-methylphenyl iodide (615-37-2) → 4-CH3C6H4BI2 (27545-47-7)

Guidance literature:

Multi-step reaction with 2 steps

1: catalyst : HI/BI₃

With catalyst : HI/BI₃;

DOI:10.1016/S0022-328X(00)87829-8

upstream raw materials:

4-tolyl iodide

p-Selenocresol

boron triiodide

toluene

Downstream raw materials:

3,5-bis(4-methylphenyl)-cyclo-1,2,4-trithia-3,5-diborolane

sulfur

tert-Butyl iodide

4-(dibromoboryl)toluene

Refernces