C₃₃H₃₃F₆N₅O₂

Base Information

Chemical Name:C₃₃H₃₃F₆N₅O₂
CAS No.:1215120-50-5
Molecular Formula:C₃₃H₃₃F₆N₅O₂
Molecular Weight:645.648
Hs Code.:

C<sub>33</sub>H<sub>33</sub>F<sub>6</sub>N<sub>5</sub>O<sub>2</sub>

Synonyms:C₃₃H₃₃F₆N₅O₂

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Chemical Property of C₃₃H₃₃F₆N₅O₂

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Technology Process of C₃₃H₃₃F₆N₅O₂

There total 6 articles about C₃₃H₃₃F₆N₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1215121-52-0
C₃₈H₄₁F₆N₅O₄

: 1215120-50-5
C₃₃H₃₃F₆N₅O₂

Guidance literature:: C₃₈H₄₁F₆N₅O₄; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 20h;

With ammonia; In dichloromethane; water; at 0 ℃;

Reference yield:

: 59-48-3
2-oxoindole

: 1215120-50-5
C₃₃H₃₃F₆N₅O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

1.2: 15 h

2.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / 0 - 20 °C

2.2: 72 h / 0 - 20 °C

3.1: hydrogen / palladium on carbon / ethanol / 24 h / 2585.81 Torr

4.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h / 0 °C

5.1: N-ethyl-N,N-diisopropylamine; 1,2-dichloro-ethane / butan-1-ol; dichloromethane / 15 h / 65 °C / Sealed tube

6.1: trifluoroacetic acid / dichloromethane / 20 h / 20 °C

6.2: 0 °C

With hydrogenchloride; hydrogen; sodium hexamethyldisilazane; potassium hexamethylsilazane; 1,2-dichloro-ethane; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on carbon; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; butan-1-ol;

Reference yield:

: 1086063-19-5
1'-benzylspiro[indoline-3,4'-piperidin]-2-one

: 1215120-50-5
C₃₃H₃₃F₆N₅O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / 0 - 20 °C

1.2: 72 h / 0 - 20 °C

2.1: hydrogen / palladium on carbon / ethanol / 24 h / 2585.81 Torr

3.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h / 0 °C

4.1: N-ethyl-N,N-diisopropylamine; 1,2-dichloro-ethane / butan-1-ol; dichloromethane / 15 h / 65 °C / Sealed tube

5.1: trifluoroacetic acid / dichloromethane / 20 h / 20 °C

5.2: 0 °C

With hydrogenchloride; hydrogen; potassium hexamethylsilazane; 1,2-dichloro-ethane; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on carbon; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; butan-1-ol;