diethyl (methylsthio)phenylmalonate

Base Information

Chemical Name:diethyl (methylsthio)phenylmalonate
CAS No.:82751-11-9
Molecular Formula:C₁₄H₁₈O₄S
Molecular Weight:282.361
Hs Code.:

Synonyms:diethyl (methylsthio)phenylmalonate

Suppliers and Price of diethyl (methylsthio)phenylmalonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl (methylsthio)phenylmalonate

Chemical Property:

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Technology Process of diethyl (methylsthio)phenylmalonate

There total 4 articles about diethyl (methylsthio)phenylmalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 2949-92-0,31761-75-8
methanethiosulfonic acid S-methyl ester

: 154377-07-8
diethyl phenyl(methylsulfonyl)malonate

: 82751-11-9
diethyl (methylsthio)phenylmalonate

Guidance literature:: diethyl phenyl(methylsulfonyl)malonate; With 1,4-diaza-bicyclo[2.2.2]octane; In toluene; at 20 ℃; for 8h; Reflux;

methanethiosulfonic acid S-methyl ester; at 20 ℃; for 6h;
DOI:10.1080/00397910902962852

Reference yield:

: 2949-92-0,31761-75-8
methanethiosulfonic acid S-methyl ester

: 83-13-6
diethyl 2-phenylmalonate

: 82751-11-9
diethyl (methylsthio)phenylmalonate

Guidance literature:: With sodium hydride; In dimethyl sulfoxide;

Reference yield:

: 101-97-3
Ethyl 2-phenylethanoate

: 82751-11-9
diethyl (methylsthio)phenylmalonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium ethoxide / ethanol / Heating

2: tetrahydrofuran / 3 h / Ambient temperature

With sodium ethanolate; In tetrahydrofuran; ethanol;
DOI:10.1246/bcsj.55.1216