(S)-α-Methoxy-α-(trifluormethyl)phenylessigsaeure-(S)-(2-methylbutyl)ester

Base Information

Chemical Name:(S)-α-Methoxy-α-(trifluormethyl)phenylessigsaeure-(S)-(2-methylbutyl)ester
CAS No.:111137-99-6
Molecular Formula:C₁₅H₁₉F₃O₃
Molecular Weight:304.309
Hs Code.:

Synonyms:(S)-α-Methoxy-α-(trifluormethyl)phenylessigsaeure-(S)-(2-methylbutyl)ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-α-Methoxy-α-(trifluormethyl)phenylessigsaeure-(S)-(2-methylbutyl)ester

Chemical Property:

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Technology Process of (S)-α-Methoxy-α-(trifluormethyl)phenylessigsaeure-(S)-(2-methylbutyl)ester

There total 12 articles about (S)-α-Methoxy-α-(trifluormethyl)phenylessigsaeure-(S)-(2-methylbutyl)ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1565-80-6
(2S)-2-methyl-1-butanol

: 20445-33-4,39637-99-5
(R)-methoxytrifluoromethylphenylacetyl chloride

: 111137-99-6
(S)-α-Methoxy-α-(trifluormethyl)phenylessigsaeure-(S)-(2-methylbutyl)ester

Guidance literature:: With pyridine; for 1.5h; Ambient temperature;

Reference yield:

: 1565-80-6
(2S)-2-methyl-1-butanol

: 17257-71-5,20445-31-2,56135-03-6,81655-41-6
(S)-Mosher acid

: 111137-99-6
(S)-α-Methoxy-α-(trifluormethyl)phenylessigsaeure-(S)-(2-methylbutyl)ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 15h; Yield given; Ambient temperature;

Reference yield:

: 111042-75-2
(1R,3R,4S)-p-menthan-3-yl hydrogen (R)-ethylmalonate

: 111137-99-6
(S)-α-Methoxy-α-(trifluormethyl)phenylessigsaeure-(S)-(2-methylbutyl)ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) (COCl)2; 2.) n-BuNBH₄ / -78 deg C

2: 1.) PPh₃+CCl₄; 2.) n-Bu₃SnH+AlBN; 3.) i-Bu₂AlH; 4.) DCC, DMAP

With tetrachloromethane; dmap; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); n-BuNBH₄; tri-n-butyl-tin hydride; diisobutylaluminium hydride; dicyclohexyl-carbodiimide; triphenylphosphine;
DOI:10.1039/c39870000619