(Z)-4,4'-Diphenyl-5,5'-bis-(5,6,7,8-tetrahydro-naphthalen-2-yl)-[2,2']bi[[1,3]dithiolylidene]

Base Information

Chemical Name:(Z)-4,4'-Diphenyl-5,5'-bis-(5,6,7,8-tetrahydro-naphthalen-2-yl)-[2,2']bi[[1,3]dithiolylidene]
CAS No.:180747-25-5
Molecular Formula:C₃₈H₃₂S₄
Molecular Weight:616.936
Hs Code.:

Synonyms:(Z)-4,4'-Diphenyl-5,5'-bis-(5,6,7,8-tetrahydro-naphthalen-2-yl)-[2,2']bi[[1,3]dithiolylidene]

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Chemical Property of (Z)-4,4'-Diphenyl-5,5'-bis-(5,6,7,8-tetrahydro-naphthalen-2-yl)-[2,2']bi[[1,3]dithiolylidene]

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Technology Process of (Z)-4,4'-Diphenyl-5,5'-bis-(5,6,7,8-tetrahydro-naphthalen-2-yl)-[2,2']bi[[1,3]dithiolylidene]

There total 7 articles about (Z)-4,4'-Diphenyl-5,5'-bis-(5,6,7,8-tetrahydro-naphthalen-2-yl)-[2,2']bi[[1,3]dithiolylidene] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 2-Ethylthio-4-(5,6,7,8-tetrahydronaphthalen-2-yl)-5-phenyl-1,3-dithioliumperchlorat

: 180747-25-5
(Z)-4,4'-Diphenyl-5,5'-bis-(5,6,7,8-tetrahydro-naphthalen-2-yl)-[2,2']bi[[1,3]dithiolylidene]

Guidance literature:: With triphenylphosphine; In acetonitrile; at 20 ℃; for 3h;

Reference yield: 53.0%

: 180746-77-4
4-(5,6,7,8-Tetrahydronaphthalen-2-yl)-5-phenyl-1,3-dithiol-2-thion

: 180747-25-5
(Z)-4,4'-Diphenyl-5,5'-bis-(5,6,7,8-tetrahydro-naphthalen-2-yl)-[2,2']bi[[1,3]dithiolylidene]

Guidance literature:: With triethyl phosphite; In xylene; at 85 ℃; for 6h;

Reference yield:

: 2-Bromo-2-phenyl-1-(5,6,7,8-tetrahydro-naphthalen-2-yl)-ethanone

: 180747-25-5
(Z)-4,4'-Diphenyl-5,5'-bis-(5,6,7,8-tetrahydro-naphthalen-2-yl)-[2,2']bi[[1,3]dithiolylidene]

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / methanol / 0.5 h / 60 °C

2: 93 percent / 70percent HClO₄ / 1 h / Heating

3: 95 percent / pyridine, H₂S / acetonitrile / 0.75 h

4: 94 percent / 0.25 h / 140 - 150 °C

5: 77 percent / PPh₃ / acetonitrile / 3 h / 20 °C

With pyridine; perchloric acid; hydrogen sulfide; triphenylphosphine; In methanol; acetonitrile;