4,8-dibenzoyl ester-1-tetralone

Base Information

• Chemical Name: 4,8-dibenzoyl ester-1-tetralone
• CAS No.: 53859-14-6
• Molecular Formula: C₂₄H₁₈O₅
• Molecular Weight: 386.404
• Mol file: 53859-14-6.mol

Synonyms:4,8-dibenzoyl ester-1-tetralone

Chemical Property of 4,8-dibenzoyl ester-1-tetralone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,8-dibenzoyl ester-1-tetralone

There total 3 articles about 4,8-dibenzoyl ester-1-tetralone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,5-dibenzoyloxytetrahydronaphthalene → 4,8-dibenzoyl ester-1-tetralone (53859-14-6)

Guidance literature:

With tert.-butylhydroperoxide; dipyridinium dichromate; In benzene; at 20 ℃; for 24h;

Reference yield:

5-Hydroxy-1-tetralone (28315-93-7) → 4,8-dibenzoyl ester-1-tetralone (53859-14-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 20 °C

2: pyridine / 20 h / 20 °C

3: dipyridinium dichromate; tert.-butylhydroperoxide / benzene / 24 h / 20 °C

With tert.-butylhydroperoxide; sodium tetrahydroborate; dipyridinium dichromate; In pyridine; methanol; benzene;

Reference yield:

→ 4,8-dibenzoyl ester-1-tetralone (53859-14-6)

Guidance literature:

Isoscleron (I), Benzoylchlorid;

upstream raw materials:

5-Hydroxy-1-tetralone

Downstream raw materials:

isosclerone

Refernces