trans-[Fe(III)(1,4,8,11-tetraazacyclotetradecane)(phenylacetylenide)₂](trifluoromethanesulfonate)

Base Information

• Chemical Name: trans-[Fe(III)(1,4,8,11-tetraazacyclotetradecane)(phenylacetylenide)₂](trifluoromethanesulfonate)
• CAS No.: 1315376-95-4
• Molecular Formula: CF₃O₃S*C₂₆H₃₄FeN₄
• Molecular Weight: 607.5

Synonyms:trans-[Fe(III)(1,4,8,11-tetraazacyclotetradecane)(phenylacetylenide)₂](trifluoromethanesulfonate)

Chemical Property of trans-[Fe(III)(1,4,8,11-tetraazacyclotetradecane)(phenylacetylenide)₂](trifluoromethanesulfonate)

Chemical Property:

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Technology Process of trans-[Fe(III)(1,4,8,11-tetraazacyclotetradecane)(phenylacetylenide)₂](trifluoromethanesulfonate)

There total 2 articles about trans-[Fe(III)(1,4,8,11-tetraazacyclotetradecane)(phenylacetylenide)₂](trifluoromethanesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

cis/trans-[Fe(III)(1,4,8,11-tetraazacyclotetradecane)(trifluoromethanesulfonate)2](trifluoromethanesulfonate)*trifluoromethanesulfonic acid + phenylacetylene (536-74-3) → trans-[Fe(III)(1,4,8,11-tetraazacyclotetradecane)(phenylacetylenide)2](trifluoromethanesulfonate) (1315376-95-4)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1021/om300515r

Reference yield: 64.0%

trans-[Fe(1,4,8,11-tetraazacyclotetradecane)(trifluoromethanesulfonate)2](trifluoromethanesulfonate) (1315376-97-6,1393729-75-3) + lithium phenylacetylide (4440-01-1) → trans-[Fe(III)(1,4,8,11-tetraazacyclotetradecane)(phenylacetylenide)2](trifluoromethanesulfonate) (1315376-95-4)

Guidance literature:

In tetrahydrofuran; Fe complex and Li compd. (4 equiv.) were reacted in THF at room temp. for 1 h;

DOI:10.1021/ic200836v

upstream raw materials:

trans-[Fe(1,4,8,11-tetraazacyclotetradecane)(trifluoromethanesulfonate)2](trifluoromethanesulfonate)

lithium phenylacetylide

phenylacetylene

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