(4-Chloro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol

Base Information

• Chemical Name: (4-Chloro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol
• CAS No.: 1544673-40-6
• Molecular Formula: C₁₃H₁₈BClO₃
• Molecular Weight: 268.548
• Mol file: 1544673-40-6.mol

Synonyms:[4-chloro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanol

Chemical Property of (4-Chloro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

2-Chloro-5-hydroxymethylphenylboronicAcid,PinacolEster ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Useful:

Technology Process of (4-Chloro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol

There total 3 articles about (4-Chloro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H16BClO3 (1112209-14-9) → [4-chloro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanol (1544673-40-6)

Guidance literature:

With sodium tetrahydroborate; at 20 ℃; for 5h;

DOI:10.3390/molecules181012346

Reference yield:

2-chloro-5-(hydroxymethyl)phenylboronic acid (1150114-78-5) → [4-chloro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanol (1544673-40-6)

Guidance literature:

Multi-step reaction with 2 steps

1: magnesium sulfate / methanol / 6 h / 20 °C

2: sodium tetrahydroborate / 5 h / 20 °C

With sodium tetrahydroborate; magnesium sulfate; In methanol;

DOI:10.3390/molecules181012346

Reference yield:

2,3-dimethyl-2,3-butane diol (76-09-5) → [4-chloro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanol (1544673-40-6)

Guidance literature:

Multi-step reaction with 2 steps

1: magnesium sulfate / methanol / 6 h / 20 °C

2: sodium tetrahydroborate / 5 h / 20 °C

With sodium tetrahydroborate; magnesium sulfate; In methanol;

DOI:10.3390/molecules181012346

upstream raw materials:

2-chloro-5-(hydroxymethyl)phenylboronic acid

C₁₃H₁₆BClO₃

2,3-dimethyl-2,3-butane diol

Downstream raw materials:

2-[4-chloro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl]isoindoline-1,3-dione

[4-chloro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanamine

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