N,N-Dimethyl-2-[(1S,6S)-6-methyl-3-((S)-2-methyl-4-oxo-butyl)-cyclohex-2-enyl]-acetamide

Base Information

Chemical Name:N,N-Dimethyl-2-[(1S,6S)-6-methyl-3-((S)-2-methyl-4-oxo-butyl)-cyclohex-2-enyl]-acetamide
CAS No.:118682-35-2
Molecular Formula:C₁₆H₂₇NO₂
Molecular Weight:265.396
Hs Code.:

Synonyms:N,N-Dimethyl-2-[(1S,6S)-6-methyl-3-((S)-2-methyl-4-oxo-butyl)-cyclohex-2-enyl]-acetamide

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Chemical Property of N,N-Dimethyl-2-[(1S,6S)-6-methyl-3-((S)-2-methyl-4-oxo-butyl)-cyclohex-2-enyl]-acetamide

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Technology Process of N,N-Dimethyl-2-[(1S,6S)-6-methyl-3-((S)-2-methyl-4-oxo-butyl)-cyclohex-2-enyl]-acetamide

There total 5 articles about N,N-Dimethyl-2-[(1S,6S)-6-methyl-3-((S)-2-methyl-4-oxo-butyl)-cyclohex-2-enyl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 118682-34-1
2-[(1S,6S)-3-((S)-4-Hydroxy-2-methyl-butyl)-6-methyl-cyclohex-2-enyl]-N,N-dimethyl-acetamide

: 118682-35-2
N,N-Dimethyl-2-[(1S,6S)-6-methyl-3-((S)-2-methyl-4-oxo-butyl)-cyclohex-2-enyl]-acetamide

Guidance literature:: With Swern oxidation;
DOI:10.1021/ja00189a037

Reference yield:

: 118713-57-8
3-Methyl-4-((S)-4-methyl-cyclohex-1-enyl)-butyric acid

: 118682-35-2
N,N-Dimethyl-2-[(1S,6S)-6-methyl-3-((S)-2-methyl-4-oxo-butyl)-cyclohex-2-enyl]-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: I₂, NaHCO₃ / acetonitrile; H₂O / 2.5 h / Ambient temperature

2: 80 percent / DBU / 105 °C

3: 96 percent / LiAlH₄

4: 2.) K₂CO₃ / 1.) xylene, 130 deg C, 18 h, 2.) CH₃OH, 2.5 h

5: 90 percent / Swern oxidation

With lithium aluminium tetrahydride; iodine; sodium hydrogencarbonate; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In water; acetonitrile;
DOI:10.1021/ja00189a037

Reference yield:

: 118682-33-0
(1S,4S)-1-((R)-4-Hydroxy-2-methyl-butyl)-4-methyl-cyclohex-2-enol

: 118682-35-2
N,N-Dimethyl-2-[(1S,6S)-6-methyl-3-((S)-2-methyl-4-oxo-butyl)-cyclohex-2-enyl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) K₂CO₃ / 1.) xylene, 130 deg C, 18 h, 2.) CH₃OH, 2.5 h

2: 90 percent / Swern oxidation

With potassium carbonate;
DOI:10.1021/ja00189a037