3-[4-(9-hydroxy-3,6-dimethoxythioxanthen-9-yl)phenyl]propionic acid N-oxysuccinimide ester

Base Information

Chemical Name:3-[4-(9-hydroxy-3,6-dimethoxythioxanthen-9-yl)phenyl]propionic acid N-oxysuccinimide ester
CAS No.:880643-72-1
Molecular Formula:C₂₈H₂₅NO₇S
Molecular Weight:519.575
Hs Code.:

Synonyms:3-[4-(9-hydroxy-3,6-dimethoxythioxanthen-9-yl)phenyl]propionic acid N-oxysuccinimide ester

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Chemical Property of 3-[4-(9-hydroxy-3,6-dimethoxythioxanthen-9-yl)phenyl]propionic acid N-oxysuccinimide ester

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Technology Process of 3-[4-(9-hydroxy-3,6-dimethoxythioxanthen-9-yl)phenyl]propionic acid N-oxysuccinimide ester

There total 4 articles about 3-[4-(9-hydroxy-3,6-dimethoxythioxanthen-9-yl)phenyl]propionic acid N-oxysuccinimide ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-[4-(9-hydroxy-3,6-dimethoxy-9H-thioxanthen-9-yl)-phenyl]-propionic acid

: 74124-79-1
di(succinimido) carbonate

: 880643-72-1
3-[4-(9-hydroxy-3,6-dimethoxythioxanthen-9-yl)phenyl]propionic acid N-oxysuccinimide ester

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; acetonitrile; at 20 ℃; for 2h;
DOI:10.1039/b504913j

Reference yield:

: 3,6-dimethoxy-9H-thioxanthen-9-one

: 880643-72-1
3-[4-(9-hydroxy-3,6-dimethoxythioxanthen-9-yl)phenyl]propionic acid N-oxysuccinimide ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: t-BuLi / pentane; tetrahydrofuran / 1 h / -80 - -40 °C

1.2: 56 percent / pentane; tetrahydrofuran / -80 - 20 °C

2.1: aq. trifluoroacetic acid / tetrahydrofuran / 1 h

2.2: LiOH / aq. ethanol / 20 °C

3.1: Et₃N / acetonitrile; dimethylformamide / 2 h / 20 °C

With tert.-butyl lithium; triethylamine; trifluoroacetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile; pentane;
DOI:10.1039/b504913j

Reference yield:

: 845272-39-1
1-[2-(4-bromophenyl)ethyl]-4-methyl-2,6,7-trioxabicyclo[2.2.2]octane

: 880643-72-1
3-[4-(9-hydroxy-3,6-dimethoxythioxanthen-9-yl)phenyl]propionic acid N-oxysuccinimide ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: t-BuLi / pentane; tetrahydrofuran / 1 h / -80 - -40 °C

1.2: 56 percent / pentane; tetrahydrofuran / -80 - 20 °C

2.1: aq. trifluoroacetic acid / tetrahydrofuran / 1 h

2.2: LiOH / aq. ethanol / 20 °C

3.1: Et₃N / acetonitrile; dimethylformamide / 2 h / 20 °C

With tert.-butyl lithium; triethylamine; trifluoroacetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile; pentane;
DOI:10.1039/b504913j