2,3,4-trimethoxy-6-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)phenol

Base Information

Chemical Name:2,3,4-trimethoxy-6-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)phenol
CAS No.:1448816-23-6
Molecular Formula:C₁₇H₁₈N₄O₅
Molecular Weight:358.354
Hs Code.:

Synonyms:2,3,4-trimethoxy-6-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)phenol

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Chemical Property of 2,3,4-trimethoxy-6-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)phenol

Chemical Property:

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Technology Process of 2,3,4-trimethoxy-6-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)phenol

There total 10 articles about 2,3,4-trimethoxy-6-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1448816-37-2
1-(2-(benzyloxy)-3,4,5-trimethoxyphenyl)-5-(4-methoxyphenyl)-1H-tetrazole

: 1448816-23-6
2,3,4-trimethoxy-6-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)phenol

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; for 7h; under 3102.97 Torr;
DOI:10.1016/j.bmcl.2013.06.004

Reference yield:

: 1448816-32-7
N-(2-(benzyloxy)-3,4,5-trimethoxyphenyl)-4-methoxybenzamide

: 1448816-23-6
2,3,4-trimethoxy-6-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol / 7 h / 3102.97 Torr

With pyridine; sodium azide; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.004

Reference yield:

: 2103-57-3
2,3,4-trimethoxybenzaldehyde

: 1448816-23-6
2,3,4-trimethoxy-6-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)phenol

Guidance literature:: Multi-step reaction with 8 steps

1.1: nitric acid / acetic acid / 1 h / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 6 h / Inert atmosphere

2.2: 4 h / Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / Inert atmosphere

4.1: tin(II) chloride dihdyrate / ethyl acetate / 20 h / 60 °C / Inert atmosphere

5.1: triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

6.1: oxalyl dichloride; pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere

7.1: sodium azide / N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere

8.1: palladium 10% on activated carbon; hydrogen / methanol / 7 h / 3102.97 Torr

With pyridine; sodium azide; oxalyl dichloride; tin(II) chloride dihdyrate; palladium 10% on activated carbon; hydrogen; nitric acid; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; acetic acid; ethyl acetate; N,N-dimethyl-formamide; 2.1: |Dakin Phenol Oxidation / 2.2: |Dakin Phenol Oxidation;
DOI:10.1016/j.bmcl.2013.06.004