2,2,6,6-tetramethylbenzo[1,2-d;4,5-d¹](bis[1,3]dioxol-4-yl)-2-(cyclohexyl)methanol

Base Information

• Chemical Name: 2,2,6,6-tetramethylbenzo[1,2-d;4,5-d¹](bis[1,3]dioxol-4-yl)-2-(cyclohexyl)methanol
• CAS No.: 1456705-28-4
• Molecular Formula: C₁₉H₂₆O₅
• Molecular Weight: 334.412

Synonyms:2,2,6,6-tetramethylbenzo[1,2-d;4,5-d¹](bis[1,3]dioxol-4-yl)-2-(cyclohexyl)methanol

Chemical Property of 2,2,6,6-tetramethylbenzo[1,2-d;4,5-d¹](bis[1,3]dioxol-4-yl)-2-(cyclohexyl)methanol

Chemical Property:

Purity/Quality:

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Technology Process of 2,2,6,6-tetramethylbenzo[1,2-d;4,5-d¹](bis[1,3]dioxol-4-yl)-2-(cyclohexyl)methanol

There total 3 articles about 2,2,6,6-tetramethylbenzo[1,2-d;4,5-d¹](bis[1,3]dioxol-4-yl)-2-(cyclohexyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,2,6,6-tetramethylbenzo[1,2-d;4,5-d1]bis[1,3]dioxole (67820-74-0) + cyclohexanecarbaldehyde (2043-61-0) → 2,2,6,6-tetramethylbenzo[1,2-d;4,5-d1](bis[1,3]dioxol-4-yl)-2-(cyclohexyl)methanol (1456705-28-4)

Guidance literature:

2,2,6,6-tetramethylbenzo[1,2-d;4,5-d¹]bis[1,3]dioxole; In tetrahydrofuran; cyclohexane; at -20 - 20 ℃; for 2.5h;

cyclohexanecarbaldehyde; In tetrahydrofuran; at 20 ℃; for 20h;

DOI:10.1016/j.ejmech.2013.06.039

Reference yield:

1,2,4,5-benzenetetrol (636-32-8) → 2,2,6,6-tetramethylbenzo[1,2-d;4,5-d1](bis[1,3]dioxol-4-yl)-2-(cyclohexyl)methanol (1456705-28-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / benzene / 1.5 h / 20 °C

2.1: tetrahydrofuran; cyclohexane / 2.5 h / -20 - 20 °C

2.2: 20 h / 20 °C

With toluene-4-sulfonic acid; In tetrahydrofuran; cyclohexane; benzene;

DOI:10.1016/j.ejmech.2013.06.039

Reference yield:

2,5-dihydroxy-1,4-benzoquinone (615-94-1) → 2,2,6,6-tetramethylbenzo[1,2-d;4,5-d1](bis[1,3]dioxol-4-yl)-2-(cyclohexyl)methanol (1456705-28-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: hydrogenchloride; tin / 1 h / 110 °C

2.1: toluene-4-sulfonic acid / benzene / 1.5 h / 20 °C

3.1: tetrahydrofuran; cyclohexane / 2.5 h / -20 - 20 °C

3.2: 20 h / 20 °C

With hydrogenchloride; tin; toluene-4-sulfonic acid; In tetrahydrofuran; cyclohexane; benzene;

DOI:10.1016/j.ejmech.2013.06.039

upstream raw materials:

1,2,4,5-benzenetetrol

2,2,6,6-tetramethylbenzo[1,2-d;4,5-d¹]bis[1,3]dioxole

cyclohexanecarbaldehyde

2,5-dihydroxy-1,4-benzoquinone

Downstream raw materials:

3-(cyclohexylmethyl)-2,5-dihydroxycyclohexa-2,5-diene-1,4-dione

2,2,6,6-tetramethylbenzo[1,2-d;4,5-d¹](bis[1,3]dioxol-4-yl)-1-methylcyclohexane

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