Technology Process of C27H22N2O4
There total 5 articles about C27H22N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium diacetate; potassium carbonate; Trimethylacetic acid;
In
N,N-dimethyl acetamide;
at 100 ℃;
for 6h;
Inert atmosphere;
DOI:10.1039/c3cc49717h
- Guidance literature:
-
Multi-step reaction with 3 steps
1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 24 h / 0 - 20 °C
2: acetonitrile / 5 h / 20 °C / Inert atmosphere; Irradiation
3: potassium carbonate; palladium diacetate; Trimethylacetic acid / N,N-dimethyl acetamide / 6 h / 100 °C / Inert atmosphere
With
palladium diacetate; potassium carbonate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; Trimethylacetic acid;
In
dichloromethane; N,N-dimethyl acetamide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c3cc49717h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetonitrile / 5 h / 20 °C / Inert atmosphere; Irradiation
2: potassium carbonate; palladium diacetate; Trimethylacetic acid / N,N-dimethyl acetamide / 6 h / 100 °C / Inert atmosphere
With
palladium diacetate; potassium carbonate; Trimethylacetic acid;
In
N,N-dimethyl acetamide; acetonitrile;
DOI:10.1039/c3cc49717h