benzyl oleanate 3-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:benzyl oleanate 3-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranoside
CAS No.:1609983-81-4
Molecular Formula:C₇₉H₈₇NO₁₃
Molecular Weight:1258.56
Hs Code.:

Synonyms:benzyl oleanate 3-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranoside

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Chemical Property of benzyl oleanate 3-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranoside

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Technology Process of benzyl oleanate 3-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranoside

There total 1 articles about benzyl oleanate 3-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1609983-78-9
6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-α-D-glucopyranoside trichloroacet-imidate

: 303114-51-4
oleanolic acid benzyl ester

: 1609983-81-4
benzyl oleanate 3-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranoside

Guidance literature:: 6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-α-D-glucopyranoside trichloroacet-imidate; oleanolic acid benzyl ester; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; for 1.5h; Molecular sieve;
DOI:10.1016/j.ejmech.2014.03.080

Reference yield:

: 1609983-81-4
benzyl oleanate 3-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranoside

: C₇₂H₈₁NO₁₃

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; dichloromethane; for 5h; under 760.051 Torr;
DOI:10.1016/j.ejmech.2014.03.080