N,N'-bis(N-benzyloxycarbonyl)-1,28-diamino-4,25-dioxa-5,24-dioxooctacosane

Base Information

Chemical Name:N,N'-bis(N-benzyloxycarbonyl)-1,28-diamino-4,25-dioxa-5,24-dioxooctacosane
CAS No.:217471-35-7
Molecular Formula:C₄₂H₆₄N₂O₈
Molecular Weight:724.979
Hs Code.:

Synonyms:N,N'-bis(N-benzyloxycarbonyl)-1,28-diamino-4,25-dioxa-5,24-dioxooctacosane

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Chemical Property of N,N'-bis(N-benzyloxycarbonyl)-1,28-diamino-4,25-dioxa-5,24-dioxooctacosane

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Technology Process of N,N'-bis(N-benzyloxycarbonyl)-1,28-diamino-4,25-dioxa-5,24-dioxooctacosane

There total 2 articles about N,N'-bis(N-benzyloxycarbonyl)-1,28-diamino-4,25-dioxa-5,24-dioxooctacosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 34637-22-4
3-[(N-benzyloxycarbonyl)amino]propanol

: 101702-50-5
1,20-eicosanedioyl dichloride

: 217471-35-7
N,N'-bis(N-benzyloxycarbonyl)-1,28-diamino-4,25-dioxa-5,24-dioxooctacosane

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/jo981195k

Reference yield:

: 2424-92-2
octadecane-1,18-dicarboxylic acid

: 217471-35-7
N,N'-bis(N-benzyloxycarbonyl)-1,28-diamino-4,25-dioxa-5,24-dioxooctacosane

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 3 h / Heating

2: 59 percent / DMAP / CH₂Cl₂ / 24 h / 20 °C

With dmap; thionyl chloride; In dichloromethane; 1: Substitution / 2: Esterification;
DOI:10.1021/jo981195k