[3-(2,4,6-trimethyl-3,5-dichlorophenyl)isoxazol-5-yl]methyl 2-chloro-3-oxobutanoate

Base Information

Chemical Name:[3-(2,4,6-trimethyl-3,5-dichlorophenyl)isoxazol-5-yl]methyl 2-chloro-3-oxobutanoate
CAS No.:271795-18-7
Molecular Formula:C₁₇H₁₆Cl₃NO₄
Molecular Weight:404.677
Hs Code.:

Synonyms:[3-(2,4,6-trimethyl-3,5-dichlorophenyl)isoxazol-5-yl]methyl 2-chloro-3-oxobutanoate

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Chemical Property of [3-(2,4,6-trimethyl-3,5-dichlorophenyl)isoxazol-5-yl]methyl 2-chloro-3-oxobutanoate

Chemical Property:

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Technology Process of [3-(2,4,6-trimethyl-3,5-dichlorophenyl)isoxazol-5-yl]methyl 2-chloro-3-oxobutanoate

There total 3 articles about [3-(2,4,6-trimethyl-3,5-dichlorophenyl)isoxazol-5-yl]methyl 2-chloro-3-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 271795-17-6
[3-(2,4,6-trimethyl-3,5-dichlorophenyl)isoxazol-5-yl]methyl 3-oxobutanoate

: 271795-18-7
[3-(2,4,6-trimethyl-3,5-dichlorophenyl)isoxazol-5-yl]methyl 2-chloro-3-oxobutanoate

Guidance literature:: With sulfuryl dichloride; sodium hydrogencarbonate; In chloroform; at 0 - 5 ℃; for 3h;
DOI:10.3987/com-99-8821

Reference yield:

: 29816-99-7
propargyl acetoacetate

: 271795-18-7
[3-(2,4,6-trimethyl-3,5-dichlorophenyl)isoxazol-5-yl]methyl 2-chloro-3-oxobutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / CCl₄ / 6 h / Heating

2: SO₂Cl₂; NaHCO₃ / CHCl₃ / 3 h / 0 - 5 °C

With sulfuryl dichloride; sodium hydrogencarbonate; In tetrachloromethane; chloroform; 1: Cycloaddition / 2: Chlorination;
DOI:10.3987/com-99-8821

Reference yield:

: 13456-86-5
3,5-Dichloro-2,4,6-trimethyl-benzonitrile N-oxide

: 271795-18-7
[3-(2,4,6-trimethyl-3,5-dichlorophenyl)isoxazol-5-yl]methyl 2-chloro-3-oxobutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / CCl₄ / 6 h / Heating

2: SO₂Cl₂; NaHCO₃ / CHCl₃ / 3 h / 0 - 5 °C

With sulfuryl dichloride; sodium hydrogencarbonate; In tetrachloromethane; chloroform; 1: Cycloaddition / 2: Chlorination;
DOI:10.3987/com-99-8821