Technology Process of C13H14FNO3
There total 7 articles about C13H14FNO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium tetrahydroborate; lithium chloride / tetrahydrofuran; ethanol / 20 °C
2: triethylamine / dichloromethane / 1 h / 0 - 20 °C
3: sodium iodide / acetone / Reflux
4: 24 h / 20 °C
5: potassium carbonate; dihydrogen peroxide / ethanol; water / 0 °C
6: Rhodococcus erythropolis AJ270 cells / acetone; aq. phosphate buffer / 2 h / 30 °C / pH 7 / Enzymatic reaction
7: methanol; diethyl ether / 1 h / -15 - 20 °C
With
sodium tetrahydroborate; dihydrogen peroxide; potassium carbonate; triethylamine; sodium iodide; lithium chloride;
In
tetrahydrofuran; methanol; aq. phosphate buffer; diethyl ether; ethanol; dichloromethane; water; acetone;
DOI:10.1016/j.tet.2014.05.018
- Guidance literature:
-
Multi-step reaction with 6 steps
1: triethylamine / dichloromethane / 1 h / 0 - 20 °C
2: sodium iodide / acetone / Reflux
3: 24 h / 20 °C
4: potassium carbonate; dihydrogen peroxide / ethanol; water / 0 °C
5: Rhodococcus erythropolis AJ270 cells / acetone; aq. phosphate buffer / 2 h / 30 °C / pH 7 / Enzymatic reaction
6: methanol; diethyl ether / 1 h / -15 - 20 °C
With
dihydrogen peroxide; potassium carbonate; triethylamine; sodium iodide;
In
methanol; aq. phosphate buffer; diethyl ether; ethanol; dichloromethane; water; acetone;
DOI:10.1016/j.tet.2014.05.018
