C₃₈H₄₄O₁₃

Base Information

Chemical Name:C₃₈H₄₄O₁₃
CAS No.:1286209-86-6
Molecular Formula:C₃₈H₄₄O₁₃
Molecular Weight:708.76
Hs Code.:

C<sub>38</sub>H<sub>44</sub>O<sub>13</sub>

Synonyms:C₃₈H₄₄O₁₃

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Chemical Property of C₃₈H₄₄O₁₃

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Technology Process of C₃₈H₄₄O₁₃

There total 6 articles about C₃₈H₄₄O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1286209-85-5
C₄₄H₅₈O₁₃Si

: 1286209-86-6
C₃₈H₄₄O₁₃

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 0 - 20 ℃; for 5h;
DOI:10.1002/chem.201003399

Reference yield:

: 1204206-79-0
C₄₃H₅₀O₁₄

: 1286209-86-6
C₃₈H₄₄O₁₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: palladium 10% on activated carbon; hydrogen; acetic acid / ethyl acetate / 24 h / 20 °C / 750.08 Torr

2.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 1.5 h / -78 - -10 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / -13 - 0 °C

3.2: -78 °C

3.3: -78 - -10 °C

4.1: dmap / dichloromethane / 16.5 h / 0 - 20 °C

5.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 3 h / Reflux

6.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 5 h / 0 - 20 °C

With dmap; n-butyllithium; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; tri-n-butyl-tin hydride; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; hexane; dichloromethane; ethyl acetate; benzene; 2.1: Swern oxidation;
DOI:10.1002/chem.201003399

Reference yield:

: C₃₆H₄₂O₁₄

: 1286209-86-6
C₃₈H₄₄O₁₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / -13 - 0 °C

1.2: -78 °C

1.3: -78 - -10 °C

2.1: dmap / dichloromethane / 16.5 h / 0 - 20 °C

3.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 3 h / Reflux

4.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 5 h / 0 - 20 °C

With dmap; n-butyllithium; 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; acetic acid; In tetrahydrofuran; hexane; dichloromethane; benzene;
DOI:10.1002/chem.201003399