(S,E)-7-((2R,5S,6S)-6-(2-methoxy-2-oxoethyl)-5-(methoxymethoxy)tetrahydro-2H-pyran-2-yl)hept-6-en-2-yl benzoate

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Chemical Name:(S,E)-7-((2R,5S,6S)-6-(2-methoxy-2-oxoethyl)-5-(methoxymethoxy)tetrahydro-2H-pyran-2-yl)hept-6-en-2-yl benzoate
CAS No.:1219981-82-4
Molecular Formula:C₂₄H₃₄O₇
Molecular Weight:434.53
Hs Code.:

Synonyms:(S,E)-7-((2R,5S,6S)-6-(2-methoxy-2-oxoethyl)-5-(methoxymethoxy)tetrahydro-2H-pyran-2-yl)hept-6-en-2-yl benzoate

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Chemical Property of (S,E)-7-((2R,5S,6S)-6-(2-methoxy-2-oxoethyl)-5-(methoxymethoxy)tetrahydro-2H-pyran-2-yl)hept-6-en-2-yl benzoate

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Technology Process of (S,E)-7-((2R,5S,6S)-6-(2-methoxy-2-oxoethyl)-5-(methoxymethoxy)tetrahydro-2H-pyran-2-yl)hept-6-en-2-yl benzoate

There total 15 articles about (S,E)-7-((2R,5S,6S)-6-(2-methoxy-2-oxoethyl)-5-(methoxymethoxy)tetrahydro-2H-pyran-2-yl)hept-6-en-2-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: C₃₉H₆₀O₇Si₂

: 1219981-82-4
(S,E)-7-((2R,5S,6S)-6-(2-methoxy-2-oxoethyl)-5-(methoxymethoxy)tetrahydro-2H-pyran-2-yl)hept-6-en-2-yl benzoate

Guidance literature:: With copper(l) iodide; tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol300200m

Reference yield: 73.0%

: 1219981-70-0
(S)-pent-4-en-2-yl benzoate

: 1219981-74-4
C₁₂H₁₉IO₅

: 1219981-82-4
(S,E)-7-((2R,5S,6S)-6-(2-methoxy-2-oxoethyl)-5-(methoxymethoxy)tetrahydro-2H-pyran-2-yl)hept-6-en-2-yl benzoate

Guidance literature:: (S)-pent-4-en-2-yl benzoate; With 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; at 0 - 20 ℃; for 1.75h;

With caesium carbonate; In tetrahydrofuran; water; at 20 ℃; for 0.583333h;

C₁₂H₁₉IO₅; With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triphenyl-arsane; In tetrahydrofuran; water; N,N-dimethyl-formamide; at 20 ℃; for 11.5h;
DOI:10.1016/j.tet.2010.07.062

Reference yield:

: 1219981-74-4
C₁₂H₁₉IO₅

: C₂₀H₂₉BO₂

: 1219981-82-4
(S,E)-7-((2R,5S,6S)-6-(2-methoxy-2-oxoethyl)-5-(methoxymethoxy)tetrahydro-2H-pyran-2-yl)hept-6-en-2-yl benzoate

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triphenyl-arsane; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 11.5h;
DOI:10.1021/ol100463a