tert-butyl (2-(2-[(2,6-dimethylphenyl)thio]-1H-indol-3-yl)ethyl)carbamate

Base Information

Chemical Name:tert-butyl (2-(2-[(2,6-dimethylphenyl)thio]-1H-indol-3-yl)ethyl)carbamate
CAS No.:1054598-83-2
Molecular Formula:C₂₃H₂₈N₂O₂S
Molecular Weight:396.554
Hs Code.:

Synonyms:tert-butyl (2-(2-[(2,6-dimethylphenyl)thio]-1H-indol-3-yl)ethyl)carbamate

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Chemical Property of tert-butyl (2-(2-[(2,6-dimethylphenyl)thio]-1H-indol-3-yl)ethyl)carbamate

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Technology Process of tert-butyl (2-(2-[(2,6-dimethylphenyl)thio]-1H-indol-3-yl)ethyl)carbamate

There total 1 articles about tert-butyl (2-(2-[(2,6-dimethylphenyl)thio]-1H-indol-3-yl)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129225-67-8
2,6-dimethylbenzenesulfenyl chloride

: 103549-24-2
tert-butyl [2-(1H-indol-3-yl)ethyl]carbamate

: 1054598-83-2
tert-butyl (2-(2-[(2,6-dimethylphenyl)thio]-1H-indol-3-yl)ethyl)carbamate

Guidance literature:: In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1002/anie.200801336

Reference yield: 89.0%

: 4-chloro-2-diazo-but-3-enoic acid ethyl ester

: 1054598-83-2
tert-butyl (2-(2-[(2,6-dimethylphenyl)thio]-1H-indol-3-yl)ethyl)carbamate

: ethyl (2E)-4-{3-{2-[(tert-butoxycarbonyl)amino]ethyl}-2-[(2,6-dimethylphenyl)sulfanyl]-3H-indol-3-yl}-4-chlorobut-2-enoate

Guidance literature:: With Rh₂(N-[(4-tert-butylphenyl)sulfonyl]-(D)-proline₎₄; In dichloromethane; at 20 ℃; for 3h; diastereospecific reaction; Inert atmosphere;
DOI:10.1002/anie.200801336