HCl*H-Thr-OAbc

Base Information

• Chemical Name: HCl*H-Thr-OAbc
• CAS No.: 144800-29-3
• Molecular Formula: C₁₈H₂₀N₄O₄*ClH
• Molecular Weight: 392.842
• Mol file: 144800-29-3.mol

Synonyms:HCl*H-Thr-OAbc

Chemical Property of HCl*H-Thr-OAbc

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of HCl*H-Thr-OAbc

There total 3 articles about HCl*H-Thr-OAbc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

Boc-Thr-OAbc (144800-38-4) → HCl*H-Thr-OAbc (144800-29-3)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 0.5h; Ambient temperature;

DOI:10.1135/cccc19921495

Reference yield:

aniline yellow (60-09-3) → HCl*H-Thr-OAbc (144800-29-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 95 percent / Na₂CO₃ / CHCl₃; H₂O

2: 85 percent / 2 M methanolic MeONa, 15-crown-5 / dimethylformamide / 0.5 h / 50 °C

3: 94 percent / 4 M HCl / dioxane / 0.5 h / Ambient temperature

With hydrogenchloride; 15-crown-5; sodium methylate; sodium carbonate; In 1,4-dioxane; chloroform; water; N,N-dimethyl-formamide;

DOI:10.1135/cccc19921495

Reference yield:

p-(bromoacetamido)azobenzene (144800-02-2) → HCl*H-Thr-OAbc (144800-29-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / 2 M methanolic MeONa, 15-crown-5 / dimethylformamide / 0.5 h / 50 °C

2: 94 percent / 4 M HCl / dioxane / 0.5 h / Ambient temperature

With hydrogenchloride; 15-crown-5; sodium methylate; In 1,4-dioxane; N,N-dimethyl-formamide;

DOI:10.1135/cccc19921495

upstream raw materials:

Boc-Thr-OAbc

aniline yellow

p-(bromoacetamido)azobenzene