[(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine-(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid]

Base Information

• Chemical Name: [(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine-(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid]
• CAS No.: 1412697-41-6
• Molecular Formula: C₄₂H₅₆N₆O₁₃
• Molecular Weight: 852.939

Synonyms:[(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine-(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid]

Chemical Property of [(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine-(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine-(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid]

There total 3 articles about [(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine-(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine-(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine methyl ester (1412697-37-0) → [(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine-(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid] (1412697-41-6)

Guidance literature:

With water; barium(II) hydroxide; In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1002/ejoc.201200463

Reference yield:

6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonic acid (668990-26-9) → [(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine-(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid] (1412697-41-6)

Guidance literature:

Multi-step reaction with 4 steps

1.1: O-(benzotriazol-1-yl )-N,N,N' ,N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.08 h

1.2: 20 h / 20 °C / Inert atmosphere

2.1: water; barium(II) hydroxide / tetrahydrofuran / 3 h / 20 °C

3.1: O-(benzotriazol-1-yl )-N,N,N' ,N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.08 h

3.2: 20 h / 20 °C / Inert atmosphere

4.1: water; barium(II) hydroxide / tetrahydrofuran / 3 h / 20 °C

With O-(benzotriazol-1-yl )-N,N,N' ,N'-tetramethyluronium tetrafluoroborate; water; barium(II) hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1002/ejoc.201200463

Reference yield:

(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine methyl ester (1412697-33-6) → [(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine-(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine acid] (1412697-41-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: O-(benzotriazol-1-yl )-N,N,N' ,N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.08 h

1.2: 20 h / 20 °C / Inert atmosphere

2.1: water; barium(II) hydroxide / tetrahydrofuran / 3 h / 20 °C

With O-(benzotriazol-1-yl )-N,N,N' ,N'-tetramethyluronium tetrafluoroborate; water; barium(II) hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1002/ejoc.201200463

upstream raw materials:

(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine methyl ester

(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine-(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine methyl ester

6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonic acid

Downstream raw materials:

(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine-(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine-(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine methyl ester

cyclo[(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine-(6-amino-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-D-phenylalanine]

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