methyl 2-(3-chlorobenzo[b]thiophene-2-carboxamido)-4-(N-(4-chlorophenyl)-N-methylcarbamoyl)benzoic acid.

Base Information

Chemical Name:methyl 2-(3-chlorobenzo[b]thiophene-2-carboxamido)-4-(N-(4-chlorophenyl)-N-methylcarbamoyl)benzoic acid.
CAS No.:1374779-31-3
Molecular Formula:C₂₅H₁₈Cl₂N₂O₄S
Molecular Weight:513.401
Hs Code.:

Synonyms:methyl 2-(3-chlorobenzo[b]thiophene-2-carboxamido)-4-(N-(4-chlorophenyl)-N-methylcarbamoyl)benzoic acid.

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Chemical Property of methyl 2-(3-chlorobenzo[b]thiophene-2-carboxamido)-4-(N-(4-chlorophenyl)-N-methylcarbamoyl)benzoic acid.

Chemical Property:

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Technology Process of methyl 2-(3-chlorobenzo[b]thiophene-2-carboxamido)-4-(N-(4-chlorophenyl)-N-methylcarbamoyl)benzoic acid.

There total 5 articles about methyl 2-(3-chlorobenzo[b]thiophene-2-carboxamido)-4-(N-(4-chlorophenyl)-N-methylcarbamoyl)benzoic acid. which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21815-91-8
3-chlorobenzo[b]thiophen-2-carbonyl chloride

: 1374779-30-2
C₁₆H₁₅ClN₂O₃

: 1374779-31-3
methyl 2-(3-chlorobenzo[b]thiophene-2-carboxamido)-4-(N-(4-chlorophenyl)-N-methylcarbamoyl)benzoic acid.

Guidance literature:: In tetrahydrofuran; for 14h; Reflux;

Reference yield:

: 35092-89-8
4-(methoxycarbonyl)-3-nitrobenzoic acid

: 1374779-31-3
methyl 2-(3-chlorobenzo[b]thiophene-2-carboxamido)-4-(N-(4-chlorophenyl)-N-methylcarbamoyl)benzoic acid.

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine; thionyl chloride / toluene / 4 h / Reflux

1.2: 14 h / 20 °C

2.1: platinum on carbon / methanol / 20 h

3.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 5 °C

3.2: 12 h / 20 °C

4.1: tetrahydrofuran / 14 h / Reflux

With pyridine; thionyl chloride; sodium hydride; platinum on carbon; In tetrahydrofuran; methanol; toluene;

Reference yield:

: 106-47-8
4-chloro-aniline

: 1374779-31-3
methyl 2-(3-chlorobenzo[b]thiophene-2-carboxamido)-4-(N-(4-chlorophenyl)-N-methylcarbamoyl)benzoic acid.

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine; thionyl chloride / toluene / 4 h / Reflux

1.2: 14 h / 20 °C

2.1: platinum on carbon / methanol / 20 h

3.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 5 °C

3.2: 12 h / 20 °C

4.1: tetrahydrofuran / 14 h / Reflux

With pyridine; thionyl chloride; sodium hydride; platinum on carbon; In tetrahydrofuran; methanol; toluene;