hexadecane-1-sulfonic acid 3,5-bis-(3,5-bis-bromomethyl-phenoxymethyl)-phenyl ester

Base Information

Chemical Name:hexadecane-1-sulfonic acid 3,5-bis-(3,5-bis-bromomethyl-phenoxymethyl)-phenyl ester
CAS No.:249630-32-8
Molecular Formula:C₄₀H₅₄Br₄O₅S
Molecular Weight:966.548
Hs Code.:

Synonyms:hexadecane-1-sulfonic acid 3,5-bis-(3,5-bis-bromomethyl-phenoxymethyl)-phenyl ester

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Chemical Property of hexadecane-1-sulfonic acid 3,5-bis-(3,5-bis-bromomethyl-phenoxymethyl)-phenyl ester

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Technology Process of hexadecane-1-sulfonic acid 3,5-bis-(3,5-bis-bromomethyl-phenoxymethyl)-phenyl ester

There total 7 articles about hexadecane-1-sulfonic acid 3,5-bis-(3,5-bis-bromomethyl-phenoxymethyl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 249630-41-9
hexadecane-1-sulfonic acid 3,5-bis-(3,5-bis-hydroxymethyl-phenoxymethyl)-phenyl ester

: 249630-32-8
hexadecane-1-sulfonic acid 3,5-bis-(3,5-bis-bromomethyl-phenoxymethyl)-phenyl ester

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1021/jo990776m

Reference yield:

: 13036-02-7
Dimethyl 5-hydroxyisophthalate

: 249630-32-8
hexadecane-1-sulfonic acid 3,5-bis-(3,5-bis-bromomethyl-phenoxymethyl)-phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / DMAP; Et₃N

2: 82 percent / KBH₄; LiCl / tetrahydrofuran

3: 85 percent / NaOH / ethanol

4: 91 percent

5: 71 percent / CBr₄; PPh₃ / tetrahydrofuran / 4 h / 20 °C

With dmap; sodium hydroxide; potassium borohydride; carbon tetrabromide; triethylamine; triphenylphosphine; lithium chloride; In tetrahydrofuran; ethanol; 1: Substitution / 2: Reduction / 3: Substitution / 4: Substitution / 5: Substitution;
DOI:10.1021/jo990776m

Reference yield:

: 249630-30-6
hexadecane-1-sulfonic acid 3,5-bis-hydroxymethyl-phenyl ester

: 249630-32-8
hexadecane-1-sulfonic acid 3,5-bis-(3,5-bis-bromomethyl-phenoxymethyl)-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / NaOH / ethanol

2: 91 percent

3: 71 percent / CBr₄; PPh₃ / tetrahydrofuran / 4 h / 20 °C

With sodium hydroxide; carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; ethanol; 1: Substitution / 2: Substitution / 3: Substitution;
DOI:10.1021/jo990776m