Technology Process of C27H24N2O8S2
There total 6 articles about C27H24N2O8S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C28H26N2O8S2;
With
sodium hydroxide; water;
In
tetrahydrofuran;
at 25 ℃;
for 60h;
With
hydrogenchloride;
In
tetrahydrofuran; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 0.5 h / 25 °C
2: pyridine; 2,6-dimethylpyridine / dichloromethane / 66 h / 25 °C
3: sodium hydroxide; water / tetrahydrofuran / 60 h / 25 °C
With
pyridine; 2,6-dimethylpyridine; sodium hydroxide; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; water;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine; magnesium chloride / 0 - 20 °C
2.1: lithium hydroxide; water / tetrahydrofuran / 5 h / 20 °C
2.2: pH 2
3.1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 0.5 h / 25 °C
4.1: pyridine; 2,6-dimethylpyridine / dichloromethane / 66 h / 25 °C
5.1: sodium hydroxide; water / tetrahydrofuran / 60 h / 25 °C
With
pyridine; 2,6-dimethylpyridine; lithium hydroxide; sodium hydroxide; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; water; triethylamine; magnesium chloride;
In
tetrahydrofuran; dichloromethane;