triethylammonium 2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl hydrogenphosphonate

Base Information

• Chemical Name: triethylammonium 2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl hydrogenphosphonate
• CAS No.: 115236-85-6
• Molecular Formula: C₆H₁₅N*C₃₄H₃₇O₈P
• Molecular Weight: 705.829

Synonyms:triethylammonium 2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl hydrogenphosphonate

Chemical Property of triethylammonium 2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl hydrogenphosphonate

Chemical Property:

Purity/Quality:

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Technology Process of triethylammonium 2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl hydrogenphosphonate

There total 2 articles about triethylammonium 2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl hydrogenphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2,3,4,6-tetra-O-benzyl-α-D-mannopyranoside (4132-28-9,4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,78609-16-2) → triethylammonium 2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl hydrogenphosphonate (115236-85-6)

Guidance literature:

With 1H-imidazole; triethylamine; phosphorus trichloride; In acetonitrile; at 20 ℃; for 0.166667h;

DOI:10.1016/0008-6215(90)84021-L

Reference yield:

2,3,4,6-tetra-O-benzyl-D-mannopyranose (4132-28-9,4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5) + triethylamine carbonate (15715-58-9) → triethylammonium 2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl hydrogenphosphonate (115236-85-6) + 2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl hydrogenphosphate triethylammonium salt (1065483-75-1)

Guidance literature:

2,3,4,6-tetra-O-benzyl-D-mannopyranose; With 1H-imidazole; triethylamine; phosphorus trichloride; In dichloromethane; at 20 ℃; for 0.333333h;

triethylamine carbonate; With water; In acetonitrile; for 0.25h; pH=7; Further stages. Title compound not separated from byproducts.;

DOI:10.1039/b000727g

Reference yield:

methyl 2,3,6-tri-O-benzoyl-β-D-galactopyranoside (34820-01-4,6344-46-3) + triethylammonium 2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl hydrogenphosphonate (115236-85-6) → methyl 2,3,6-tri-O-benzoyl-β-D-galactopyranoside 4-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl phosphate), triethylammonium salt (125177-49-3,131150-21-5)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1016/0008-6215(90)84021-L

upstream raw materials:

2,3,4,6-tetra-O-benzyl-α-D-mannopyranoside

2,3,4,6-tetra-O-benzyl-D-mannopyranose

triethylamine carbonate

Downstream raw materials:

methyl 2,3,6-tri-O-benzoyl-β-D-galactopyranoside 4-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl phosphate), triethylammonium salt

methyl 2,3,6-tri-O-benzoyl-α-D-mannopyranoside 4-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl-phosphate), triethylammonium salt

methyl 3,4,6-tri-O-benzoyl-α-D-mannopyranoside 2-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl-phosphate), triethylammonium salt

methyl 2,4,6-tri-O-benzoyl-α-D-mannopyranoside 3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl-phosphate), triethylammonium salt

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