methyl-(η1-dppm)-bis(μ-dppm)-diplatinum iodide

Base Information

Chemical Name:methyl-(η1-dppm)-bis(μ-dppm)-diplatinum iodide
CAS No.:84190-20-5
Molecular Formula:C₇₆H₆₉P₆Pt₂*I
Molecular Weight:1685.29
Hs Code.:

Synonyms:methyl-(η1-dppm)-bis(μ-dppm)-diplatinum iodide

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Chemical Property of methyl-(η1-dppm)-bis(μ-dppm)-diplatinum iodide

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Technology Process of methyl-(η1-dppm)-bis(μ-dppm)-diplatinum iodide

There total 1 articles about methyl-(η1-dppm)-bis(μ-dppm)-diplatinum iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: Pt2(μ-bis(diphenylphosphino)methane)3

: 84190-20-5
methyl-(η1-dppm)-bis(μ-dppm)-diplatinum iodide

Guidance literature:: With methyl iodide; In benzene; MeI in benzene was added under N2 to a soln. of Pt-complex in benzene in a Schlenk tube, mixt. was stirred at room temp. for 3.5 h; ppt. was recovered by filtration, washed with benzene, dried in vacuo;
DOI:10.1021/om00083a009

Reference yield: 84.0%

: 17084-13-8
potassium hexafluorophosphate

: 84190-20-5
methyl-(η1-dppm)-bis(μ-dppm)-diplatinum iodide

: 84190-22-7
Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3⁽¹⁺⁾*PF₆^(1-)=(Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3)PF₆

Guidance literature:: In dichloromethane; water; a soln. of KPF6 in water was added to a CH2Cl2 soln. of Pt-complex, mixt. was stirred for 45 min; org. phase was sepd., washed with water, dried (molecular sieve), cyclohexane was added slowly, crystals were recovered by filtration and driedin vacuo; elem. anal. for the adduct with 0.35 CH2Cl2;
DOI:10.1021/om00083a009