C₃₅H₅₉N₃O₈Si₂

Base Information

• Chemical Name: C₃₅H₅₉N₃O₈Si₂
• CAS No.: 1231975-21-5
• Molecular Formula: C₃₅H₅₉N₃O₈Si₂
• Molecular Weight: 706.04
• Mol file: 1231975-21-5.mol

Synonyms:C₃₅H₅₉N₃O₈Si₂

Chemical Property of C₃₅H₅₉N₃O₈Si₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₃₅H₅₉N₃O₈Si₂

There total 12 articles about C₃₅H₅₉N₃O₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C43H63N3O10Si2 (1231975-35-1) → C35H59N3O8Si2 (1231975-21-5)

Guidance literature:

C₄₃H₆₃N₃O₁₀Si₂; With (-)-1,2-bis-((2R,5R)-2,5-dimethylphospholano)benzene-(cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; In methanol; for 336h; under 750.075 Torr;

With palladium 10% on activated carbon; hydrogen; In methanol; for 5h; under 750.075 Torr; diastereoselective reaction;

DOI:10.1021/jo201935w

Reference yield: 66.0%

C35H57N3O9Si2 (1346620-39-0) + p-methoxybenzyl chloride (824-94-2) → C35H59N3O8Si2 (1231975-21-5)

Guidance literature:

C₃₅H₅₇N₃O₉Si₂; p-methoxybenzyl chloride; With tetra-(n-butyl)ammonium iodide; sodium carbonate; In dichloromethane; water; at 20 ℃; for 30h;

With cyclohexa-1,4-diene; palladium 10% on activated carbon; In methanol; at 20 ℃; for 3h;

DOI:10.1021/jo201935w

Reference yield: 28.0%

C40H67N3O10Si2 (1231975-32-8) → C35H59N3O8Si2 (1231975-21-5)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 20 ℃; for 72h;

DOI:10.1039/c003092a

upstream raw materials:

C₄₃H₆₅N₃O₁₀Si₂

C₄₀H₆₇N₃O₁₀Si₂

2',3',5'-tris(O-tert-butyldimethylsilyl)-3-(p-methoxybenzyl)uridine

C₄₃H₆₃N₃O₁₀Si₂

Downstream raw materials:

C₅₂H₈₃N₅O₁₁Si₂