tBu₂PhSiPH₂

Base Information

Chemical Name:tBu₂PhSiPH₂
CAS No.:751478-16-7
Molecular Formula:C₁₄H₂₅PSi
Molecular Weight:252.412
Hs Code.:

Synonyms:tBu₂PhSiPH₂

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Chemical Property of tBu₂PhSiPH₂

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Technology Process of tBu₂PhSiPH₂

There total 1 articles about tBu₂PhSiPH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 140903-06-6
di-tert-butylchlorophenylsilane

: 751478-16-7
tBu₂PhSiPH₂

Guidance literature:: With lithium dihydrogenphosphide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/b921473a

Reference yield: 50.0%

: 751478-16-7
tBu₂PhSiPH₂

: 55681-99-7
tri-tert-butyl gallium

: [tBu₂GaP(H)SitBu₂Ph]₂

Guidance literature:: In n-heptane; at 60 ℃; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c7dt00950j

Reference yield: 38.0%

: 751478-16-7
tBu₂PhSiPH₂

: 55147-78-9
bis(bis(trimethylsilyl)amido)tin(II)

: 1356938-46-9
Sn₄P₄(tBu₂PhSi)4

Guidance literature:: In tetrahydrofuran; under dry Ar; tBu2PhSiPH2 dissolved in THF, at -74°C Sn(N(SiMe3)2)2 added; left to warm to room temp. slowly; stirred overnight; soln. concd.; left at 4°C; elem. anal.;
DOI:10.1002/zaac.201100217