N-(5-aminopentyl)-2-(((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl)thio)benzamide

Base Information

• Chemical Name: N-(5-aminopentyl)-2-(((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl)thio)benzamide
• CAS No.: 1402249-29-9
• Molecular Formula: C₂₇H₄₂N₂OS
• Molecular Weight: 442.709
• Mol file: 1402249-29-9.mol

Synonyms:N-(5-aminopentyl)-2-(((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl)thio)benzamide

Chemical Property of N-(5-aminopentyl)-2-(((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl)thio)benzamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(5-aminopentyl)-2-(((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl)thio)benzamide

There total 1 articles about N-(5-aminopentyl)-2-(((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl)thio)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-tert-butoxycarbonylamino-1-aminopentane (51644-96-3) → N-(5-aminopentyl)-2-(((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl)thio)benzamide (1402249-29-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 4-methyl-morpholine; chloroformic acid ethyl ester / tetrahydrofuran / 1 h / 0 °C

1.2: 1 h / 0 °C

2.1: trifluoroacetic acid / dichloromethane / 20 °C

With 4-methyl-morpholine; chloroformic acid ethyl ester; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;

DOI:10.1111/cbdd.12393

Reference yield:

acetic acid 4-(2-chlorocarbonylvinyl)phenyl ester + N-(5-aminopentyl)-2-(((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl)thio)benzamide (1402249-29-9) → C38H50N2O4S

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 ℃; for 1h;

DOI:10.1111/cbdd.12393

Reference yield:

4-acetoxyferuloyl chloride (55882-65-0,108608-07-7,50906-12-2) + N-(5-aminopentyl)-2-(((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl)thio)benzamide (1402249-29-9) → C39H52N2O5S

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 ℃; for 1h;

DOI:10.1111/cbdd.12393

upstream raw materials:

5-tert-butoxycarbonylamino-1-aminopentane