10-Brom-1,8-bis<4-<1,2-dibrom-2-(3,5-di-tert-butylphenyl)ethyl>phenyl>anthracen

Base Information

Chemical Name:10-Brom-1,8-bis<4-<1,2-dibrom-2-(3,5-di-tert-butylphenyl)ethyl>phenyl>anthracen
CAS No.:140834-25-9
Molecular Formula:C₅₈H₆₁Br₅
Molecular Weight:1157.64
Hs Code.:

Synonyms:10-Brom-1,8-bis<4-<1,2-dibrom-2-(3,5-di-tert-butylphenyl)ethyl>phenyl>anthracen

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Chemical Property of 10-Brom-1,8-bis<4-<1,2-dibrom-2-(3,5-di-tert-butylphenyl)ethyl>phenyl>anthracen

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Technology Process of 10-Brom-1,8-bis<4-<1,2-dibrom-2-(3,5-di-tert-butylphenyl)ethyl>phenyl>anthracen

There total 1 articles about 10-Brom-1,8-bis<4-<1,2-dibrom-2-(3,5-di-tert-butylphenyl)ethyl>phenyl>anthracen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 140834-24-8,140834-33-9
1,8-Bis<4-<2-(3,5-di-tert-butylphenyl)ethenyl>phenyl>anthracen

: 140834-25-9
10-Brom-1,8-bis<4-<1,2-dibrom-2-(3,5-di-tert-butylphenyl)ethyl>phenyl>anthracen

Guidance literature:: With bromine; In tetrachloromethane; for 40h; Ambient temperature;

Reference yield: 12.3%

: 140834-25-9
10-Brom-1,8-bis<4-<1,2-dibrom-2-(3,5-di-tert-butylphenyl)ethyl>phenyl>anthracen

: 140834-26-0
10-Brom-1,8-bis<4-<(3,5-di-tert-butylphenyl)ethinyl>phenyl>anthracen

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 4h; Heating;

Reference yield:

: 140834-25-9
10-Brom-1,8-bis<4-<1,2-dibrom-2-(3,5-di-tert-butylphenyl)ethyl>phenyl>anthracen

: 140834-27-1
1,8-Bis<4-<(3,5-di-tert-butylphenyl)ethinyl>phenyl>anthracen

Guidance literature:: Multi-step reaction with 2 steps

1: 12.3 percent / KO-t-Bu / tetrahydrofuran / 4 h / Heating

2: 51 percent / HCO₂Na / Pd(Ph₃)4 / dimethylformamide / 1 h / 90 °C

With potassium tert-butylate; sodium formate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; N,N-dimethyl-formamide;