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Technology Process of (CH2CH2NCH2COOH)2(CH2CH2NCH2C(O)NH2CH2C6H5)(1+)*CF3CO2(1-)=[C19H29N4O5][CF3CO2]

(CH2CH2NCH2COOH)2(CH2CH2NCH2C(O)NH2CH2C6H5)(1+)*CF3CO2(1-)=[C19H29N4O5][CF3CO2]

Base Information
  • Chemical Name:(CH2CH2NCH2COOH)2(CH2CH2NCH2C(O)NH2CH2C6H5)(1+)*CF3CO2(1-)=[C19H29N4O5][CF3CO2]
  • CAS No.:1262392-71-1
  • Molecular Formula:C2HF3O2*C19H28N4O5
  • Molecular Weight:506.479
  • Hs Code.:
(CH<sub>2</sub>CH<sub>2</sub>NCH<sub>2</sub>COOH)2(CH<sub>2</sub>CH<sub>2</sub>NCH<sub>2</sub>C(O)NH<sub>2</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)<sup>(1+)</sup>*CF<sub>3</sub>CO<sub>2</sub><sup>(1-)</sup>=[C<sub>19</sub>H<sub>29</sub>N<sub>4</sub>O<sub>5</sub>][CF<sub>3</sub>CO<sub>2</sub>]

Synonyms:(CH2CH2NCH2COOH)2(CH2CH2NCH2C(O)NH2CH2C6H5)(1+)*CF3CO2(1-)=[C19H29N4O5][CF3CO2]

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Chemical Property of (CH2CH2NCH2COOH)2(CH2CH2NCH2C(O)NH2CH2C6H5)(1+)*CF3CO2(1-)=[C19H29N4O5][CF3CO2]
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Technology Process of (CH2CH2NCH2COOH)2(CH2CH2NCH2C(O)NH2CH2C6H5)(1+)*CF3CO2(1-)=[C19H29N4O5][CF3CO2]

There total 1 articles about (CH2CH2NCH2COOH)2(CH2CH2NCH2C(O)NH2CH2C6H5)(1+)*CF3CO2(1-)=[C19H29N4O5][CF3CO2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C<sub>27</sub>H<sub>44</sub>N<sub>4</sub>O<sub>5</sub>
1262392-67-5

C27H44N4O5

trifluoroacetic acid
76-05-1

trifluoroacetic acid

(CH<sub>2</sub>CH<sub>2</sub>NCH<sub>2</sub>COOH)2(CH<sub>2</sub>CH<sub>2</sub>NCH<sub>2</sub>C(O)NH<sub>2</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)<sup>(1+)</sup>*CF<sub>3</sub>CO<sub>2</sub><sup>(1-)</sup>=[C<sub>19</sub>H<sub>29</sub>N<sub>4</sub>O<sub>5</sub>][CF<sub>3</sub>CO<sub>2</sub>]
1262392-71-1

(CH2CH2NCH2COOH)2(CH2CH2NCH2C(O)NH2CH2C6H5)(1+)*CF3CO2(1-)=[C19H29N4O5][CF3CO2]

Guidance literature:
In dichloromethane; at 20 ℃; for 20h;
DOI:10.1002/ejic.201000748

Reference yield: 66.0%

gallium(III) nitrate hydrate

gallium(III) nitrate hydrate

(CH<sub>2</sub>CH<sub>2</sub>NCH<sub>2</sub>COOH)2(CH<sub>2</sub>CH<sub>2</sub>NCH<sub>2</sub>C(O)NH<sub>2</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)<sup>(1+)</sup>*CF<sub>3</sub>CO<sub>2</sub><sup>(1-)</sup>=[C<sub>19</sub>H<sub>29</sub>N<sub>4</sub>O<sub>5</sub>][CF<sub>3</sub>CO<sub>2</sub>]
1262392-71-1

(CH2CH2NCH2COOH)2(CH2CH2NCH2C(O)NH2CH2C6H5)(1+)*CF3CO2(1-)=[C19H29N4O5][CF3CO2]

water
7732-18-5

water

[Ga(CH<sub>2</sub>CH<sub>2</sub>NCH<sub>2</sub>COO)2(CH<sub>2</sub>CH<sub>2</sub>NCH<sub>2</sub>C(O)NCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)]*H<sub>2</sub>O

[Ga(CH2CH2NCH2COO)2(CH2CH2NCH2C(O)NCH2C6H5)]*H2O

Guidance literature:
With Na2CO3; In water; 1:1 mixt in H2O, pH 5 (aq. Na2CO3), refluxed for 15 min; filtered, HPLC, recrystd. (EtOH, room temp.);
DOI:10.1002/ejic.201000748

Reference yield: 66.0%

gallium(III) nitrate hydrate

gallium(III) nitrate hydrate

(CH<sub>2</sub>CH<sub>2</sub>NCH<sub>2</sub>COOH)2(CH<sub>2</sub>CH<sub>2</sub>NCH<sub>2</sub>C(O)NH<sub>2</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)<sup>(1+)</sup>*CF<sub>3</sub>CO<sub>2</sub><sup>(1-)</sup>=[C<sub>19</sub>H<sub>29</sub>N<sub>4</sub>O<sub>5</sub>][CF<sub>3</sub>CO<sub>2</sub>]
1262392-71-1

(CH2CH2NCH2COOH)2(CH2CH2NCH2C(O)NH2CH2C6H5)(1+)*CF3CO2(1-)=[C19H29N4O5][CF3CO2]

water
7732-18-5

water

trifluoroacetic acid
76-05-1

trifluoroacetic acid

[Ga(CH<sub>2</sub>CH<sub>2</sub>NCH<sub>2</sub>COO)2(CH<sub>2</sub>CH<sub>2</sub>NCH<sub>2</sub>C(O)NCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)]*CF<sub>3</sub>COOH*H<sub>2</sub>O

[Ga(CH2CH2NCH2COO)2(CH2CH2NCH2C(O)NCH2C6H5)]*CF3COOH*H2O

Guidance literature:
With Na2CO3; In water; 1:1 mixt in H2O, pH 3 (aq. Na2CO3), refluxed for 15 min; filtered, HPLC, recrystd. (EtOH, room temp.);
DOI:10.1002/ejic.201000748
upstream raw materials:

C27H44N4O5

trifluoroacetic acid

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