4-(2-methoxyphenyl)pentanoic acid

Base Information

Chemical Name:4-(2-methoxyphenyl)pentanoic acid
CAS No.:15148-43-3
Molecular Formula:C₁₂H₁₆O₃
Molecular Weight:208.257
Hs Code.:

Synonyms:4-(2-methoxyphenyl)pentanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(2-methoxyphenyl)pentanoic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 4-(2-methoxyphenyl)pentanoic acid

There total 13 articles about 4-(2-methoxyphenyl)pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 4-(2-methoxyphenyl)pentanenitrile

: 15148-43-3
4-(2-methoxyphenyl)pentanoic acid

Guidance literature:: With water; potassium hydroxide; In ethanol; for 48h; Inert atmosphere; Reflux;
DOI:10.1039/c4cc05923a

Reference yield:

: 15149-95-8
5-(2-methoxy-phenyl)-5-methyl-dihydro-furan-2-one

: 15148-43-3
4-(2-methoxyphenyl)pentanoic acid

Guidance literature:: With perchloric acid; hydrogen; palladium on activated charcoal; In acetic acid;
DOI:10.1016/0040-4020(67)80084-X

Reference yield:

: 579-74-8
2-Methoxyacetophenone

: 15148-43-3
4-(2-methoxyphenyl)pentanoic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 2.08 h / 0 °C / Inert atmosphere

1.2: Inert atmosphere; Reflux

2.1: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 20 °C / 2250.23 - 3000.3 Torr / Inert atmosphere

3.1: lithium aluminium tetrahydride / diethyl ether / 2 h / -40 °C / Inert atmosphere

4.1: pyridine / dichloromethane / 24 h / 20 °C / Inert atmosphere

5.1: potassium iodide / N,N-dimethyl-formamide / 24 h / 60 °C / Inert atmosphere

6.1: potassium hydroxide; water / ethanol / 48 h / Inert atmosphere; Reflux

With pyridine; lithium aluminium tetrahydride; palladium 10% on activated carbon; water; hydrogen; sodium hydride; potassium iodide; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c4cc05923a