(3-(3-carbamoyl-1H-pyrrol-1-yl)phenoxycarbonyl)(2-(2-phenoxyethoxy)ethyl)amine

Base Information

Chemical Name:(3-(3-carbamoyl-1H-pyrrol-1-yl)phenoxycarbonyl)(2-(2-phenoxyethoxy)ethyl)amine
CAS No.:1392287-83-0
Molecular Formula:C₂₂H₂₃N₃O₅
Molecular Weight:409.442
Hs Code.:

Synonyms:(3-(3-carbamoyl-1H-pyrrol-1-yl)phenoxycarbonyl)(2-(2-phenoxyethoxy)ethyl)amine

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Chemical Property of (3-(3-carbamoyl-1H-pyrrol-1-yl)phenoxycarbonyl)(2-(2-phenoxyethoxy)ethyl)amine

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Technology Process of (3-(3-carbamoyl-1H-pyrrol-1-yl)phenoxycarbonyl)(2-(2-phenoxyethoxy)ethyl)amine

There total 5 articles about (3-(3-carbamoyl-1H-pyrrol-1-yl)phenoxycarbonyl)(2-(2-phenoxyethoxy)ethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1245740-12-8
1-(3-hydroxyphenyl)-1H-pyrrole-3-carboxamide

: 1392288-10-6
2-(2-phenoxyethoxy)ethanisocyanate

: 1392287-83-0
(3-(3-carbamoyl-1H-pyrrol-1-yl)phenoxycarbonyl)(2-(2-phenoxyethoxy)ethyl)amine

Guidance literature:: With triethylamine; In tetrahydrofuran; at 25 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jm300689c

Reference yield:

: 81644-23-7
2,5-dimethoxytetrahydrofuran-3-carbonitrile

: 1392287-83-0
(3-(3-carbamoyl-1H-pyrrol-1-yl)phenoxycarbonyl)(2-(2-phenoxyethoxy)ethyl)amine

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / 1,4-dioxane; water / Inert atmosphere; Reflux

2: dihydrogen peroxide; sodium hydroxide / water / 12 h / Inert atmosphere; Reflux

3: triethylamine / tetrahydrofuran / 16 h / 25 °C / Inert atmosphere

With hydrogenchloride; dihydrogen peroxide; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1021/jm300689c

Reference yield:

: 104-68-7,9004-78-8
2-(2-phenoxyethoxy)ethanol

: 1392287-83-0
(3-(3-carbamoyl-1H-pyrrol-1-yl)phenoxycarbonyl)(2-(2-phenoxyethoxy)ethyl)amine

Guidance literature:: Multi-step reaction with 4 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

2.1: hydrazine hydrate / ethanol / Inert atmosphere; Reflux

3.1: sodium hydrogencarbonate / dichloromethane; water / 0.17 h / 0 °C / Inert atmosphere

3.2: 0.25 h / Inert atmosphere

4.1: triethylamine / tetrahydrofuran / 16 h / 25 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; sodium hydrogencarbonate; hydrazine hydrate; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; water; 1.1: Mitsunobu reaction;
DOI:10.1021/jm300689c