2,3-Dihydrolysergine

Base Information

Chemical Name:2,3-Dihydrolysergine
CAS No.:114249-74-0
Molecular Formula:C16H20N2
Molecular Weight:240.34
Hs Code.:

Synonyms:2,3-dihydrolysergine

Suppliers and Price of 2,3-Dihydrolysergine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-Dihydrolysergine

Chemical Property:

PSA：15.27000
LogP:3.00880

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3-Dihydrolysergine

There total 15 articles about 2,3-Dihydrolysergine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 99499-55-5
(3β,8α)-9,10-Didehydro-2,3-dihydro-1-<(4-methoxyphenyl)sulfonyl>-6,8-dimethylergoline

: 99499-56-6,114249-74-0,114249-75-1
(3β)-2,3-Dihydroisolysergine

Guidance literature:: With lithium aluminium tetrahydride; In 1,2-dimethoxyethane; for 5h; Heating;
DOI:10.1248/cpb.39.23

Reference yield: 49.0%

: 519-10-8
6,8-dimethyl-9,10-didehydro-ergoline

: 114249-74-0
(3β)-2,3-dihydrolysergine

Guidance literature:: With triethylsilane; trifluoroacetic acid; for 16h; Ambient temperature;
DOI:10.1021/jm00403a007

Reference yield:

: 99499-51-1,99546-35-7,101978-97-6
(3β,8α,9α)-2,3-Dihydro-1-<(4-methoxyphenyl)sulfonyl>-6,8-dimethylergolin-9-ol

: 99499-56-6,114249-74-0,114249-75-1
(3β)-2,3-Dihydroisolysergine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / Ambient temperature

2: 52 percent / potassium tert-butoxide / dimethylsulfoxide

3: 76 percent / LiAlH₄ / 1,2-dimethoxy-ethane

With lithium aluminium tetrahydride; potassium tert-butylate; In pyridine; 1,2-dimethoxyethane; dimethyl sulfoxide;