(1S,11S)-(+)-1-amino-1,11-diphenyl-13-(6-methylpyridyl)-12-aza-3,6,9-trioxatridecane

Base Information

Chemical Name:(1S,11S)-(+)-1-amino-1,11-diphenyl-13-(6-methylpyridyl)-12-aza-3,6,9-trioxatridecane
CAS No.:143331-40-2
Molecular Formula:C₂₇H₃₅N₃O₃
Molecular Weight:449.593
Hs Code.:

Synonyms:(1S,11S)-(+)-1-amino-1,11-diphenyl-13-(6-methylpyridyl)-12-aza-3,6,9-trioxatridecane

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Chemical Property of (1S,11S)-(+)-1-amino-1,11-diphenyl-13-(6-methylpyridyl)-12-aza-3,6,9-trioxatridecane

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Technology Process of (1S,11S)-(+)-1-amino-1,11-diphenyl-13-(6-methylpyridyl)-12-aza-3,6,9-trioxatridecane

There total 4 articles about (1S,11S)-(+)-1-amino-1,11-diphenyl-13-(6-methylpyridyl)-12-aza-3,6,9-trioxatridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 143331-39-9
(4S,14S)-4,14-Diphenyl-3,15-bis-(toluene-4-sulfonyl)-6,9,12-trioxa-3,15,21-triaza-bicyclo[15.3.1]henicosa-1⁽²⁰⁾,17⁽²¹⁾,18-triene

: 143331-40-2
(1S,11S)-(+)-1-amino-1,11-diphenyl-13-(6-methylpyridyl)-12-aza-3,6,9-trioxatridecane

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 24h; Heating;
DOI:10.1021/jo00046a020

Reference yield:

: 112633-26-8
2,6-bis[(tosyloxy)methyl]pyridine

: 143331-40-2
(1S,11S)-(+)-1-amino-1,11-diphenyl-13-(6-methylpyridyl)-12-aza-3,6,9-trioxatridecane

Guidance literature:: Multi-step reaction with 2 steps

1: 20 percent / Cs₂CO₃ / dimethylformamide / 72 h / 80 °C

2: 48 percent / LiAlH₄ / tetrahydrofuran / 24 h / Heating

With lithium aluminium tetrahydride; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo00046a020

Reference yield:

: 143331-36-6
(1S,1'S)-2,2'-((oxybis(ethane-2,1-diyl))bis(oxy))bis(1-phenylethan-1-amine)

: 143331-40-2
(1S,11S)-(+)-1-amino-1,11-diphenyl-13-(6-methylpyridyl)-12-aza-3,6,9-trioxatridecane

Guidance literature:: Multi-step reaction with 3 steps

1: 43 percent / pyridine / 1 h / 45 °C

2: 20 percent / Cs₂CO₃ / dimethylformamide / 72 h / 80 °C

3: 48 percent / LiAlH₄ / tetrahydrofuran / 24 h / Heating

With pyridine; lithium aluminium tetrahydride; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo00046a020