1-(2',3',4',6'-tetra-O-acetyl-3'-C-cyano-β-D-glucopyranosyl)-N4-benzoylcytosine

Base Information

Chemical Name:1-(2',3',4',6'-tetra-O-acetyl-3'-C-cyano-β-D-glucopyranosyl)-N4-benzoylcytosine
CAS No.:1345963-30-5
Molecular Formula:C₂₆H₂₆N₄O₁₁
Molecular Weight:570.513
Hs Code.:

Synonyms:1-(2',3',4',6'-tetra-O-acetyl-3'-C-cyano-β-D-glucopyranosyl)-N4-benzoylcytosine

Suppliers and Price of 1-(2',3',4',6'-tetra-O-acetyl-3'-C-cyano-β-D-glucopyranosyl)-N4-benzoylcytosine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(2',3',4',6'-tetra-O-acetyl-3'-C-cyano-β-D-glucopyranosyl)-N4-benzoylcytosine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(2',3',4',6'-tetra-O-acetyl-3'-C-cyano-β-D-glucopyranosyl)-N4-benzoylcytosine

There total 4 articles about 1-(2',3',4',6'-tetra-O-acetyl-3'-C-cyano-β-D-glucopyranosyl)-N4-benzoylcytosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 26661-13-2
4-N-benzoylcytosine

: 1345963-23-6
1,2,3,4,6-penta-O-acetyl-3-C-cyano-D-glucopyranose

: 1345963-30-5
1-(2',3',4',6'-tetra-O-acetyl-3'-C-cyano-β-D-glucopyranosyl)-N4-benzoylcytosine

Guidance literature:: 4-N-benzoylcytosine; With 1,1,1,3,3,3-hexamethyl-disilazane; saccharin; In acetonitrile; Inert atmosphere; Reflux;

1,2,3,4,6-penta-O-acetyl-3-C-cyano-D-glucopyranose; With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; Inert atmosphere; Reflux;

With sodium hydrogencarbonate; In water; acetonitrile;
DOI:10.1016/j.ejmech.2011.08.033

Reference yield:

: 3-C-cyano-D-glucopyranose

: 1345963-30-5
1-(2',3',4',6'-tetra-O-acetyl-3'-C-cyano-β-D-glucopyranosyl)-N4-benzoylcytosine

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 1 h / 20 °C

2.1: 1,1,1,3,3,3-hexamethyl-disilazane; saccharin / acetonitrile / Inert atmosphere; Reflux

2.2: Inert atmosphere; Reflux

With pyridine; 1,1,1,3,3,3-hexamethyl-disilazane; saccharin; In acetonitrile;
DOI:10.1016/j.ejmech.2011.08.033

Reference yield:

: 2847-00-9
1,2:5,6-di-O-isopropylidene-α-D-hexofuran-3-ulose

: 1345963-30-5
1-(2',3',4',6'-tetra-O-acetyl-3'-C-cyano-β-D-glucopyranosyl)-N4-benzoylcytosine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate / diethyl ether; water / 20 °C

2.1: water / methanol / Reflux

3.1: pyridine / 1 h / 20 °C

4.1: 1,1,1,3,3,3-hexamethyl-disilazane; saccharin / acetonitrile / Inert atmosphere; Reflux

4.2: Inert atmosphere; Reflux

With pyridine; water; sodium hydrogencarbonate; 1,1,1,3,3,3-hexamethyl-disilazane; saccharin; In methanol; diethyl ether; water; acetonitrile;
DOI:10.1016/j.ejmech.2011.08.033