C₆₄H₇₈O₁₃

Base Information

Chemical Name:C₆₄H₇₈O₁₃
CAS No.:465518-95-0
Molecular Formula:C₆₄H₇₈O₁₃
Molecular Weight:1055.32
Hs Code.:

C<sub>64</sub>H<sub>78</sub>O<sub>13</sub>

Synonyms:C₆₄H₇₈O₁₃

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Chemical Property of C₆₄H₇₈O₁₃

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Technology Process of C₆₄H₇₈O₁₃

There total 7 articles about C₆₄H₇₈O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 465518-94-9
(3R,9R)-3,9-Bis-((2R,3R,4S,5R,6R)-3-acetoxy-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-decanoic acid isopropyl ester

: 465518-95-0
C₆₄H₇₈O₁₃

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/ja036521e

Reference yield:

: 932-56-9
2-methyl-cycloheptanone

: 465518-95-0
C₆₄H₇₈O₁₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: 74 percent / aq. mCPBA / CH₂Cl₂ / 20 h / Heating

2.1: porcine liver esteraze; NaOH / aq. phosphate buffer / pH 7.2

3.1: carbonyl diimidazole / tetrahydrofuran / 4 h / 0 °C

3.2: 74 percent / tetrahydrofuran / cooling

4.1: 99 percent / [((R)-BINAP)RuCl₂]2*NEt₃; H₂ / methanol; tetrahydrofuran / 15 h / 65 °C / 15001.5 Torr

5.1: molecular sieves 4 Angstroem / CH₂Cl₂ / 0.5 h / 20 °C

5.2: 82 percent / TMSOTf / CH₂Cl₂ / 2.5 h / -78 °C

6.1: 82 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

With sodium hydroxide; lithium aluminium tetrahydride; [((R)-Binap)-RuCl₂]2; 4 A molecular sieve; porcine liver esteraze; hydrogen; 3-chloro-benzenecarboperoxoic acid; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; phosphate buffer; dichloromethane;
DOI:10.1021/ja027346p

Reference yield:

: 119434-02-5
(-)-7(R)-hydroxyoctanoic acid

: 465518-95-0
C₆₄H₇₈O₁₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: carbonyl diimidazole / tetrahydrofuran / 4 h / 0 °C

1.2: 74 percent / tetrahydrofuran / cooling

2.1: 99 percent / [((R)-BINAP)RuCl₂]2*NEt₃; H₂ / methanol; tetrahydrofuran / 15 h / 65 °C / 15001.5 Torr

3.1: molecular sieves 4 Angstroem / CH₂Cl₂ / 0.5 h / 20 °C

3.2: 82 percent / TMSOTf / CH₂Cl₂ / 2.5 h / -78 °C

4.1: 82 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

With lithium aluminium tetrahydride; [((R)-Binap)-RuCl₂]2; 4 A molecular sieve; hydrogen; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja027346p