(E)-1-[3-diphenylphosphino-2-(indolin-1-yl)benzaldehyde]-N,N-dimethylhydrazone

Base Information

Chemical Name:(E)-1-[3-diphenylphosphino-2-(indolin-1-yl)benzaldehyde]-N,N-dimethylhydrazone
CAS No.:749904-70-9
Molecular Formula:C₂₉H₂₈N₃P
Molecular Weight:449.535
Hs Code.:

Synonyms:(E)-1-[3-diphenylphosphino-2-(indolin-1-yl)benzaldehyde]-N,N-dimethylhydrazone

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Chemical Property of (E)-1-[3-diphenylphosphino-2-(indolin-1-yl)benzaldehyde]-N,N-dimethylhydrazone

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Technology Process of (E)-1-[3-diphenylphosphino-2-(indolin-1-yl)benzaldehyde]-N,N-dimethylhydrazone

There total 4 articles about (E)-1-[3-diphenylphosphino-2-(indolin-1-yl)benzaldehyde]-N,N-dimethylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 749904-56-1
(E)-1-[3-fluoro-2-(indolin-1-yl)benzaldehyde]-N,N-dimethylhydrazone

: 15475-27-1,4346-39-8
potassium diphenylphosphine

: 749904-70-9
(E)-1-[3-diphenylphosphino-2-(indolin-1-yl)benzaldehyde]-N,N-dimethylhydrazone

Guidance literature:: In tetrahydrofuran; at 55 ℃; for 24h;
DOI:10.1021/jo061261f

Reference yield:

: 749904-42-5
(E)-1-(2,3-difluorobenzaldehyde)-N,N-dimethylhydrazone

: 749904-70-9
(E)-1-[3-diphenylphosphino-2-(indolin-1-yl)benzaldehyde]-N,N-dimethylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 0.17 h / -78 °C

1.2: 96 percent / tetrahydrofuran; hexane / 24 h / 20 °C

2.1: 97 percent / tetrahydrofuran / 24 h / 55 °C

With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1021/jo061261f

Reference yield:

: 496-15-1
1-indoline

: 749904-70-9
(E)-1-[3-diphenylphosphino-2-(indolin-1-yl)benzaldehyde]-N,N-dimethylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 0.17 h / -78 °C

1.2: 96 percent / tetrahydrofuran; hexane / 24 h / 20 °C

2.1: 97 percent / tetrahydrofuran / 24 h / 55 °C

With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1021/jo061261f