C₄₁H₅₈O₉

Base Information

Chemical Name:C₄₁H₅₈O₉
CAS No.:676620-38-5
Molecular Formula:C₄₁H₅₈O₉
Molecular Weight:694.906
Hs Code.:

C<sub>41</sub>H<sub>58</sub>O<sub>9</sub>

Synonyms:C₄₁H₅₈O₉

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Chemical Property of C₄₁H₅₈O₉

Chemical Property:

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Technology Process of C₄₁H₅₈O₉

There total 5 articles about C₄₁H₅₈O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 2039-82-9
1-bromo-4-ethenyl-benzene

: 676620-25-0
C₃₃H₅₀O₉

: 676620-38-5
C₄₁H₅₈O₉

Guidance literature:: 1-bromo-4-ethenyl-benzene; With tert.-butyl lithium; In diethyl ether; hexane; for 0.5h;

C₃₃H₅₀O₉; In tetrahydrofuran; diethyl ether; hexane; at -78 ℃; for 0.5h; Further stages.;
DOI:10.1021/jm020461q

Reference yield:

: 63968-64-9
C₁₂H₁₃O₂(CH₃)3(O)(OO)

: 676620-38-5
C₄₁H₅₈O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: DIBAL / CH₂Cl₂; toluene / -78 °C

2.1: 1.60 g / pyridine; DMAP / CH₂Cl₂; toluene / 3 h / -78 - 20 °C

3.1: 76 percent / SnCl₄ / CH₂Cl₂ / 1 h / -78 °C

4.1: 70 percent / OsO₄; oxone / dimethylformamide; 2-methyl-propan-2-ol / 2 h

5.1: t-BuLi / diethyl ether; hexane / 0.5 h

5.2: 74 percent / tetrahydrofuran; diethyl ether; hexane / 0.5 h / -78 °C

With pyridine; dmap; Oxone; osmium(VIII) oxide; tert.-butyl lithium; tin(IV) chloride; diisobutylaluminium hydride; In diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1021/jm020461q

Reference yield:

: 81496-81-3
dihydroartesiminin

: 676620-38-5
C₄₁H₅₈O₉

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1.60 g / pyridine; DMAP / CH₂Cl₂; toluene / 3 h / -78 - 20 °C

2.1: 76 percent / SnCl₄ / CH₂Cl₂ / 1 h / -78 °C

3.1: 70 percent / OsO₄; oxone / dimethylformamide; 2-methyl-propan-2-ol / 2 h

4.1: t-BuLi / diethyl ether; hexane / 0.5 h

4.2: 74 percent / tetrahydrofuran; diethyl ether; hexane / 0.5 h / -78 °C

With pyridine; dmap; Oxone; osmium(VIII) oxide; tert.-butyl lithium; tin(IV) chloride; In diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1021/jm020461q