methyl 2-(3-chloro-4-(6-(2,4-dichlorophenylsulfonamido)-2-methyl-3H-benzo[d]imidazol-5-yloxy)phenyl)acetate

Base Information

Chemical Name:methyl 2-(3-chloro-4-(6-(2,4-dichlorophenylsulfonamido)-2-methyl-3H-benzo[d]imidazol-5-yloxy)phenyl)acetate
CAS No.:1080522-49-1
Molecular Formula:C₂₃H₁₈Cl₃N₃O₅S
Molecular Weight:554.838
Hs Code.:

Synonyms:methyl 2-(3-chloro-4-(6-(2,4-dichlorophenylsulfonamido)-2-methyl-3H-benzo[d]imidazol-5-yloxy)phenyl)acetate

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Chemical Property of methyl 2-(3-chloro-4-(6-(2,4-dichlorophenylsulfonamido)-2-methyl-3H-benzo[d]imidazol-5-yloxy)phenyl)acetate

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Technology Process of methyl 2-(3-chloro-4-(6-(2,4-dichlorophenylsulfonamido)-2-methyl-3H-benzo[d]imidazol-5-yloxy)phenyl)acetate

There total 9 articles about methyl 2-(3-chloro-4-(6-(2,4-dichlorophenylsulfonamido)-2-methyl-3H-benzo[d]imidazol-5-yloxy)phenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1080522-48-0
methyl 2-(3-chloro-4-(6-(2,4-dichlorophenylsulfonamido)-2-methyl-3-((2-(trimethylsilyl)ethoxy)methyl)-3H-benzo[d]imidazol-5-yloxy)phenyl)acetate

: 1080522-49-1
methyl 2-(3-chloro-4-(6-(2,4-dichlorophenylsulfonamido)-2-methyl-3H-benzo[d]imidazol-5-yloxy)phenyl)acetate

Guidance literature:: methyl 2-(3-chloro-4-(6-(2,4-dichlorophenylsulfonamido)-2-methyl-3-((2-(trimethylsilyl)ethoxy)methyl)-3H-benzo[d]imidazol-5-yloxy)phenyl)acetate; With trifluoroacetic acid; In dichloromethane; at 20 ℃;

With sodium hydrogencarbonate; In dichloromethane; water; ethyl acetate;

Reference yield:

: 1080522-40-2
6-fluoro-2-methyl-5-nitro-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[d]imidazole

: 1080522-49-1
methyl 2-(3-chloro-4-(6-(2,4-dichlorophenylsulfonamido)-2-methyl-3H-benzo[d]imidazol-5-yloxy)phenyl)acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: caesium carbonate / dimethyl sulfoxide / 80 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.08 h / 20 °C

2.2: 16 h / 20 °C

3.1: water; tin(ll) chloride / ethyl acetate / 2.5 h / 20 °C

4.1: pyridine / 16 h / 20 °C

5.1: trifluoroacetic acid / dichloromethane / 20 °C

With pyridine; water; caesium carbonate; trifluoroacetic acid; tin(ll) chloride; In dichloromethane; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 367-31-7
4-fluoro-1,2-phenylenediamine

: 1080522-49-1
methyl 2-(3-chloro-4-(6-(2,4-dichlorophenylsulfonamido)-2-methyl-3H-benzo[d]imidazol-5-yloxy)phenyl)acetate

Guidance literature:: Multi-step reaction with 8 steps

1.1: hydrogenchloride / ethanol; water / 0.5 h / 50 °C / Heating / reflux

1.2: 20 °C

2.1: sulfuric acid; nitric acid / 1 h / 0 °C

2.2: 0 °C

3.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C

3.2: 0 - 20 °C

4.1: caesium carbonate / dimethyl sulfoxide / 80 °C

5.1: caesium carbonate / N,N-dimethyl-formamide / 0.08 h / 20 °C

5.2: 16 h / 20 °C

6.1: water; tin(ll) chloride / ethyl acetate / 2.5 h / 20 °C

7.1: pyridine / 16 h / 20 °C

8.1: trifluoroacetic acid / dichloromethane / 20 °C

With pyridine; hydrogenchloride; sulfuric acid; water; nitric acid; sodium hydride; caesium carbonate; trifluoroacetic acid; tin(ll) chloride; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;