di-(o-iodophenyl) disulfide

Base Information

• Chemical Name: di-(o-iodophenyl) disulfide
• CAS No.: 87797-73-7
• Molecular Formula: C₁₂H₈I₂S₂
• Molecular Weight: 470.137
• Mol file: 87797-73-7.mol

Synonyms:di-(o-iodophenyl) disulfide

Chemical Property of di-(o-iodophenyl) disulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of di-(o-iodophenyl) disulfide

There total 3 articles about di-(o-iodophenyl) disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1,2-bis(o-iodophenylthio)ethane (87797-72-6) → di-(o-iodophenyl) disulfide (87797-73-7)

Guidance literature:

With aluminum oxide; at 200 ℃;

Reference yield:

2-iodobenzene-1-sulfonyl chloride (63059-29-0) → di-(o-iodophenyl) disulfide (87797-73-7)

Guidance literature:

With hydrogen iodide; acetic acid;

DOI:10.1039/jr9560001665

Reference yield:

1-chloro-(o-iodophenylthio)ethane (87797-71-5) → di-(o-iodophenyl) disulfide (87797-73-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 32 percent / alumina / 1 h / 120 °C

2: 95 percent / alumina / 200 °C

With aluminum oxide;

upstream raw materials:

2-iodobenzene-1-sulfonyl chloride

1,2-bis(o-iodophenylthio)ethane

1-chloro-(o-iodophenylthio)ethane

Downstream raw materials:

C₁₈H₂₂INO₄S₂

C₁₆H₁₇ClINO₃S₂

C₁₆H₁₇ClINO₃S₂

Thianthrene

Refernces