C₃₅H₃₉NO₂Si

Base Information

Chemical Name:C₃₅H₃₉NO₂Si
CAS No.:1620230-80-9
Molecular Formula:C₃₅H₃₉NO₂Si
Molecular Weight:533.786
Hs Code.:

C<sub>35</sub>H<sub>39</sub>NO<sub>2</sub>Si

Synonyms:C₃₅H₃₉NO₂Si

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Chemical Property of C₃₅H₃₉NO₂Si

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Technology Process of C₃₅H₃₉NO₂Si

There total 6 articles about C₃₅H₃₉NO₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620230-79-6
C₃₅H₄₁NO₃Si

: 1620230-80-9
C₃₅H₃₉NO₂Si

Guidance literature:: With dmap; methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 ℃; for 0.0833333h;
DOI:10.1039/c4cc04555f

Reference yield:

: 16077-10-4
N-benzyl-5-methoxyisatin

: 1620230-80-9
C₃₅H₃₉NO₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tetrahydroborate / ethanol / 0 - 20 °C

2.1: dmap / dichloromethane / 0.5 h / 0 °C

3.1: triethylamine; formaldehyd / dichloromethane / 4 h / 20 °C

3.2: 3 h / 20 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 20 h / 20 °C / Inert atmosphere

5.1: tetrahydrofuran; diethyl ether / 1 h / 0 °C / Inert atmosphere

5.2: 3 h / Inert atmosphere; Reflux

6.1: methanesulfonyl chloride; triethylamine; dmap / dichloromethane / 0.08 h / 0 °C

With 1H-imidazole; dmap; sodium tetrahydroborate; formaldehyd; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c4cc04555f

Reference yield:

: 1620230-77-4
1-benzyl-3-hydroxy-3-(hydroxymethyl)-5-methoxyindolin-2-one

: 1620230-80-9
C₃₅H₃₉NO₂Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 20 h / 20 °C / Inert atmosphere

2.1: tetrahydrofuran; diethyl ether / 1 h / 0 °C / Inert atmosphere

2.2: 3 h / Inert atmosphere; Reflux

3.1: methanesulfonyl chloride; triethylamine; dmap / dichloromethane / 0.08 h / 0 °C

With 1H-imidazole; dmap; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c4cc04555f