4-[2-(4-fluorobutoxy)ethyl][bis(4-methoxymethoxyphenyl)methylene]cyclohexane

Base Information

Chemical Name:4-[2-(4-fluorobutoxy)ethyl][bis(4-methoxymethoxyphenyl)methylene]cyclohexane
CAS No.:886587-95-7
Molecular Formula:C₂₉H₃₉FO₅
Molecular Weight:486.624
Hs Code.:

Synonyms:4-[2-(4-fluorobutoxy)ethyl][bis(4-methoxymethoxyphenyl)methylene]cyclohexane

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Chemical Property of 4-[2-(4-fluorobutoxy)ethyl][bis(4-methoxymethoxyphenyl)methylene]cyclohexane

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Technology Process of 4-[2-(4-fluorobutoxy)ethyl][bis(4-methoxymethoxyphenyl)methylene]cyclohexane

There total 6 articles about 4-[2-(4-fluorobutoxy)ethyl][bis(4-methoxymethoxyphenyl)methylene]cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 886587-66-2
4-(2-hydroxyethyl)[bis(4-methoxymethoxyphenyl)methylene]cyclohexane

: 462-72-6
4-bromo-1-fluorobutane

: 886587-95-7
4-[2-(4-fluorobutoxy)ethyl][bis(4-methoxymethoxyphenyl)methylene]cyclohexane

Guidance literature:: 4-(2-hydroxyethyl)[bis(4-methoxymethoxyphenyl)methylene]cyclohexane; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃;

4-bromo-1-fluorobutane; In N,N-dimethyl-formamide; at 100 ℃; for 24h;
DOI:10.1021/jm0512037

Reference yield:

: 91158-10-0
4-(Carbomethoxymethylene)cyclohexanone

: 886587-95-7
4-[2-(4-fluorobutoxy)ethyl][bis(4-methoxymethoxyphenyl)methylene]cyclohexane

Guidance literature:: Multi-step reaction with 5 steps

1.1: 50 percent / H₂ / Pd/C / ethanol / 6 h / 20 °C

2.1: 71 percent / zinc; titanium(IV) chloride / tetrahydrofuran / 2 h / Heating

3.1: sodium hydride / dimethylformamide / cooling

3.2: 97 percent / dimethylformamide / 1 h / 20 °C

4.1: 96 percent / LiAlH₄ / tetrahydrofuran / 1 h / 20 °C

5.1: sodium hydride / dimethylformamide / 0 °C

5.2: 26 percent / dimethylformamide / 24 h / 100 °C

With lithium aluminium tetrahydride; hydrogen; titanium tetrachloride; sodium hydride; zinc; palladium on activated charcoal; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; 2.1: McMurry coupling;
DOI:10.1021/jm0512037

Reference yield:

: 637-88-7
1,4-Cyclohexanedione

: 886587-95-7
4-[2-(4-fluorobutoxy)ethyl][bis(4-methoxymethoxyphenyl)methylene]cyclohexane

Guidance literature:: Multi-step reaction with 6 steps

1.1: 88 percent / toluene / 8 h / 110 °C

2.1: 50 percent / H₂ / Pd/C / ethanol / 6 h / 20 °C

3.1: 71 percent / zinc; titanium(IV) chloride / tetrahydrofuran / 2 h / Heating

4.1: sodium hydride / dimethylformamide / cooling

4.2: 97 percent / dimethylformamide / 1 h / 20 °C

5.1: 96 percent / LiAlH₄ / tetrahydrofuran / 1 h / 20 °C

6.1: sodium hydride / dimethylformamide / 0 °C

6.2: 26 percent / dimethylformamide / 24 h / 100 °C

With lithium aluminium tetrahydride; hydrogen; titanium tetrachloride; sodium hydride; zinc; palladium on activated charcoal; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene; 1.1: Wittig reaction / 3.1: McMurry coupling;
DOI:10.1021/jm0512037