5-acetamido-2,6-anhydro-2-O-(N-(carbobenzyloxy)-8-amino-5-oxaoctyl)-3,5-dideoxy-D-glycero-D-galacto-α-nonulopyranosonic acid

Base Information

Chemical Name:5-acetamido-2,6-anhydro-2-O-(N-(carbobenzyloxy)-8-amino-5-oxaoctyl)-3,5-dideoxy-D-glycero-D-galacto-α-nonulopyranosonic acid
CAS No.:156857-72-6
Molecular Formula:C₂₆H₄₀N₂O₁₂
Molecular Weight:572.61
Hs Code.:

Synonyms:5-acetamido-2,6-anhydro-2-O-(N-(carbobenzyloxy)-8-amino-5-oxaoctyl)-3,5-dideoxy-D-glycero-D-galacto-α-nonulopyranosonic acid

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Chemical Property of 5-acetamido-2,6-anhydro-2-O-(N-(carbobenzyloxy)-8-amino-5-oxaoctyl)-3,5-dideoxy-D-glycero-D-galacto-α-nonulopyranosonic acid

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Technology Process of 5-acetamido-2,6-anhydro-2-O-(N-(carbobenzyloxy)-8-amino-5-oxaoctyl)-3,5-dideoxy-D-glycero-D-galacto-α-nonulopyranosonic acid

There total 3 articles about 5-acetamido-2,6-anhydro-2-O-(N-(carbobenzyloxy)-8-amino-5-oxaoctyl)-3,5-dideoxy-D-glycero-D-galacto-α-nonulopyranosonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 156847-61-9
methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2,6-anhydro-2-O-(N-(carbobenzyloxy)-8-amino-5-oxaoctyl)-3,5-dideoxy-D-glycero-D-galacto-α-nonulopyranosonate

: 156857-72-6
5-acetamido-2,6-anhydro-2-O-(N-(carbobenzyloxy)-8-amino-5-oxaoctyl)-3,5-dideoxy-D-glycero-D-galacto-α-nonulopyranosonic acid

Guidance literature:: With sodium hydroxide; at 25 ℃; for 2h;
DOI:10.1021/jm00046a027

Reference yield:

: 67670-69-3
N-acetyl-4,7,8,9-tetra-O-acetyl-2-chloro-2-deoxyneuraminic acid methyl ester

: 156857-72-6
5-acetamido-2,6-anhydro-2-O-(N-(carbobenzyloxy)-8-amino-5-oxaoctyl)-3,5-dideoxy-D-glycero-D-galacto-α-nonulopyranosonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: silver salicylate, molecular sieves 4 Angstroem / benzene / 96 h / 25 °C

2: 43 percent / 2N NaOH / 2 h / 25 °C

With sodium hydroxide; 4 A molecular sieve; silver salicylate; In benzene;
DOI:10.1021/jm00046a027

Reference yield:

: 131566-49-9
[3-(4-Hydroxy-butoxy)-propyl]-carbamic acid benzyl ester

: 156857-72-6
5-acetamido-2,6-anhydro-2-O-(N-(carbobenzyloxy)-8-amino-5-oxaoctyl)-3,5-dideoxy-D-glycero-D-galacto-α-nonulopyranosonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: silver salicylate, molecular sieves 4 Angstroem / benzene / 96 h / 25 °C

2: 43 percent / 2N NaOH / 2 h / 25 °C

With sodium hydroxide; 4 A molecular sieve; silver salicylate; In benzene;
DOI:10.1021/jm00046a027