6,7-bisbenzyloxy-1-(3,4-bisbenzyloxybenzyl)-1,2,3,4-tetrahydroisoquinoline hydrochloride

Base Information

Chemical Name:6,7-bisbenzyloxy-1-(3,4-bisbenzyloxybenzyl)-1,2,3,4-tetrahydroisoquinoline hydrochloride
CAS No.:79832-14-7
Molecular Formula:C₄₄H₄₁NO₄*ClH
Molecular Weight:684.275
Hs Code.:

Synonyms:6,7-bisbenzyloxy-1-(3,4-bisbenzyloxybenzyl)-1,2,3,4-tetrahydroisoquinoline hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6,7-bisbenzyloxy-1-(3,4-bisbenzyloxybenzyl)-1,2,3,4-tetrahydroisoquinoline hydrochloride

Chemical Property:

Purity/Quality:

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Technology Process of 6,7-bisbenzyloxy-1-(3,4-bisbenzyloxybenzyl)-1,2,3,4-tetrahydroisoquinoline hydrochloride

There total 7 articles about 6,7-bisbenzyloxy-1-(3,4-bisbenzyloxybenzyl)-1,2,3,4-tetrahydroisoquinoline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1932-43-0
6,7-bisbenzyloxy-1-(3,4-bisbenzyloxybenzyl)-3,4-dihydroisoquinoline hydrochloride

: 79832-14-7
6,7-bisbenzyloxy-1-(3,4-bisbenzyloxybenzyl)-1,2,3,4-tetrahydroisoquinoline hydrochloride

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.75h;
DOI:10.1039/P19810002016

Reference yield:

: 1699-54-3
3,4-bis(benzyloxy)-β-nitrostyrene

: 79832-14-7
6,7-bisbenzyloxy-1-(3,4-bisbenzyloxybenzyl)-1,2,3,4-tetrahydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / lithium aluminium hydride / tetrahydrofuran / 1.25 h / Heating

2: sodium hydrogen carbonate / CH₂Cl₂; H₂O / 1.5 h

3: 85 percent / phosphorus oxychloride / acetonitrile / 0.42 h / Heating

4: 92 percent / sodium borohydride / methanol / 0.75 h / 0 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; sodium hydrogencarbonate; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1039/P19810002016

Reference yield:

: 1699-61-2
<3,4-bis(benzyloxy)phenyl>acetic acid

: 79832-14-7
6,7-bisbenzyloxy-1-(3,4-bisbenzyloxybenzyl)-1,2,3,4-tetrahydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl chloride, DMF / benzene / 1 h / 20 °C

2: sodium hydrogen carbonate / CH₂Cl₂; H₂O / 1.5 h

3: 85 percent / phosphorus oxychloride / acetonitrile / 0.42 h / Heating

4: 92 percent / sodium borohydride / methanol / 0.75 h / 0 °C

With sodium tetrahydroborate; oxalyl dichloride; sodium hydrogencarbonate; N,N-dimethyl-formamide; trichlorophosphate; In methanol; dichloromethane; water; acetonitrile; benzene;
DOI:10.1039/P19810002016