Technology Process of C26H26BrN3O7S2
There total 4 articles about C26H26BrN3O7S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridinium hydrobromide perbromide;
In
dichloromethane;
at 0 - 20 ℃;
optical yield given as %ee;
Inert atmosphere;
DOI:10.1021/ja804738b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium on carbon; hydrogen / methanol / 23 °C
2: triethylamine / dichloromethane / 0 - 23 °C
3: pyridinium perbromide hydrobromide / dichloromethane / 0 - 23 °C
With
pyridinium perbromide hydrobromide; palladium on carbon; hydrogen; triethylamine;
In
methanol; dichloromethane;
DOI:10.1016/j.tetlet.2010.11.074
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tributylphosphine; di-isopropyl azodicarboxylate; ammonia / toluene / -78 - -20 °C
2: palladium on carbon; hydrogen / methanol / 23 °C
3: triethylamine / dichloromethane / 0 - 23 °C
4: pyridinium perbromide hydrobromide / dichloromethane / 0 - 23 °C
With
pyridinium perbromide hydrobromide; tributylphosphine; di-isopropyl azodicarboxylate; palladium on carbon; ammonia; hydrogen; triethylamine;
In
methanol; dichloromethane; toluene;
1: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2010.11.074