2,2-bis(benzyloxymethyl)-1,3-bis[O-β-D-galactopyranosyl-(1->4)-(2-amino-2-deoxy-β-D-glucopyranosyl-oxy)]-propane butane 1N,4N'-dioyl amide

Base Information

Chemical Name:2,2-bis(benzyloxymethyl)-1,3-bis[O-β-D-galactopyranosyl-(1->4)-(2-amino-2-deoxy-β-D-glucopyranosyl-oxy)]-propane butane 1N,4N'-dioyl amide
CAS No.:592529-56-1
Molecular Formula:C₄₇H₆₈N₂O₂₄
Molecular Weight:1045.06
Hs Code.:

Synonyms:2,2-bis(benzyloxymethyl)-1,3-bis[O-β-D-galactopyranosyl-(1->4)-(2-amino-2-deoxy-β-D-glucopyranosyl-oxy)]-propane butane 1N,4N'-dioyl amide

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Chemical Property of 2,2-bis(benzyloxymethyl)-1,3-bis[O-β-D-galactopyranosyl-(1->4)-(2-amino-2-deoxy-β-D-glucopyranosyl-oxy)]-propane butane 1N,4N'-dioyl amide

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Technology Process of 2,2-bis(benzyloxymethyl)-1,3-bis[O-β-D-galactopyranosyl-(1->4)-(2-amino-2-deoxy-β-D-glucopyranosyl-oxy)]-propane butane 1N,4N'-dioyl amide

There total 2 articles about 2,2-bis(benzyloxymethyl)-1,3-bis[O-β-D-galactopyranosyl-(1->4)-(2-amino-2-deoxy-β-D-glucopyranosyl-oxy)]-propane butane 1N,4N'-dioyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 952585-00-1
uridine-5'-diphosphoglucose

: 592529-54-9
2,2-bis(benzyloxymethyl)-1,3-bis(2-amino-2-deoxy-β-D-glucopyranosyl-oxy)-propane butane 1N,4N'-dioyl amide

: 2,2-bis-benzyloxymethyl-1-(O-2-acetamido-2-deoxy-β-D-glucopyranosyl-oxy)-3-[O-β-D-galactopyranosyl-(1->4)-(2-amino-2-deoxy-β-D-glucopyranosyl-oxy)]-propane butane-1N,4N'-dioyl amide

: 592529-56-1
2,2-bis(benzyloxymethyl)-1,3-bis[O-β-D-galactopyranosyl-(1->4)-(2-amino-2-deoxy-β-D-glucopyranosyl-oxy)]-propane butane 1N,4N'-dioyl amide

Guidance literature:: With bovine milk D-GlcNAc β-(1->4)-galactosyltransferase; UDP-glucose-4-epimerase; sodium cacodylate; manganese(ll) chloride; In water; at 37 ℃; for 96h; pH=7.4; Enzymatic reaction;
DOI:10.1016/S0008-6215(03)00129-0

Reference yield:

: 592529-48-1
2,2-bis(benzyloxymethyl)-1,3-bis(3,4,6-tri-O-acetyl-2-amino-2-deoxy-β-D-glucopyranosyl-oxy)-propane butane 1N,4N'-dioyl amide

: 592529-56-1
2,2-bis(benzyloxymethyl)-1,3-bis[O-β-D-galactopyranosyl-(1->4)-(2-amino-2-deoxy-β-D-glucopyranosyl-oxy)]-propane butane 1N,4N'-dioyl amide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / water; triethylamine / methanol / 24 h / 20 °C

2: 70 percent / bovine milk D-GlcNAc β-(1->4)-galactosyltransferase; UDP-glucose-4-epimerase; sodium cacodylate / MnCl2 / H2O / 96 h / 37 °C / pH 7.4 / Enzymatic reaction

With bovine milk D-GlcNAc β-(1->4)-galactosyltransferase; UDP-glucose-4-epimerase; water; sodium cacodylate; triethylamine; manganese(ll) chloride; In methanol; water;
DOI:10.1016/S0008-6215(03)00129-0