carboxymethyl 2-acetamido-3-O-acetyl-6-azido-4-O-benzyl-2-deoxy-α-D-glucopyranoside

Base Information

• Chemical Name: carboxymethyl 2-acetamido-3-O-acetyl-6-azido-4-O-benzyl-2-deoxy-α-D-glucopyranoside
• CAS No.: 251324-22-8
• Molecular Formula: C₁₉H₂₄N₄O₈
• Molecular Weight: 436.422
• Mol file: 251324-22-8.mol

Synonyms:carboxymethyl 2-acetamido-3-O-acetyl-6-azido-4-O-benzyl-2-deoxy-α-D-glucopyranoside

Chemical Property of carboxymethyl 2-acetamido-3-O-acetyl-6-azido-4-O-benzyl-2-deoxy-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of carboxymethyl 2-acetamido-3-O-acetyl-6-azido-4-O-benzyl-2-deoxy-α-D-glucopyranoside

There total 2 articles about carboxymethyl 2-acetamido-3-O-acetyl-6-azido-4-O-benzyl-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

Acetic acid (2S,3R,4R,5R,6R)-3-acetylamino-6-azidomethyl-5-benzyloxy-2-(2-oxo-ethoxy)-tetrahydro-pyran-4-yl ester (313479-75-3) → carboxymethyl 2-acetamido-3-O-acetyl-6-azido-4-O-benzyl-2-deoxy-α-D-glucopyranoside (251324-22-8)

Guidance literature:

With jones reagent; In acetone; for 0.5h; sonication;

DOI:10.1021/jo001183a

Reference yield: 67.0%

allyl 2-acetamido-3-O-acetyl-6-azido-4-O-benzyl-2-deoxy-α-D-glucopyranoside (251324-21-7) → Acetic acid (2S,3R,4R,5R,6R)-3-acetylamino-6-azidomethyl-5-benzyloxy-2-(2-oxo-ethoxy)-tetrahydro-pyran-4-yl ester (313479-75-3) + carboxymethyl 2-acetamido-3-O-acetyl-6-azido-4-O-benzyl-2-deoxy-α-D-glucopyranoside (251324-22-8)

Guidance literature:

With ruthenium trichloride; sodium periodate; In tetrachloromethane; water; at 20 ℃; for 2h;

DOI:10.1021/jo001183a

Reference yield: 83.0%

carboxymethyl 2-acetamido-3-O-acetyl-6-azido-4-O-benzyl-2-deoxy-α-D-glucopyranoside (251324-22-8) → carboxymethyl 2-acetamido-6-azido-4-O-benzyl-2-deoxy-α-D-glucopyranoside

Guidance literature:

With sodium methylate; In methanol; at 20 ℃; for 0.75h;

DOI:10.1021/jo001183a

upstream raw materials:

Acetic acid (2S,3R,4R,5R,6R)-3-acetylamino-6-azidomethyl-5-benzyloxy-2-(2-oxo-ethoxy)-tetrahydro-pyran-4-yl ester

allyl 2-acetamido-3-O-acetyl-6-azido-4-O-benzyl-2-deoxy-α-D-glucopyranoside