phenylmethyl 6-deoxy-3,4-O-(1-methylidene)-2-O-(phenylmethyl)-α-D-galactopyranoside

Base Information

Chemical Name:phenylmethyl 6-deoxy-3,4-O-(1-methylidene)-2-O-(phenylmethyl)-α-D-galactopyranoside
CAS No.:150650-42-3
Molecular Formula:C₂₃H₂₈O₅
Molecular Weight:384.472
Hs Code.:

Synonyms:phenylmethyl 6-deoxy-3,4-O-(1-methylidene)-2-O-(phenylmethyl)-α-D-galactopyranoside

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Chemical Property of phenylmethyl 6-deoxy-3,4-O-(1-methylidene)-2-O-(phenylmethyl)-α-D-galactopyranoside

Chemical Property:

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Technology Process of phenylmethyl 6-deoxy-3,4-O-(1-methylidene)-2-O-(phenylmethyl)-α-D-galactopyranoside

There total 4 articles about phenylmethyl 6-deoxy-3,4-O-(1-methylidene)-2-O-(phenylmethyl)-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6189-71-5
α-D-fucose

: 150650-42-3
phenylmethyl 6-deoxy-3,4-O-(1-methylidene)-2-O-(phenylmethyl)-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / CSA

2: 84 percent / TsOH / acetone / 1 h / 25 °C

3: 1.) NaH, imidazole, 2.) n-Bu₄NI / 1.) THF, from 0 to 25 deg C, 50 min, 2.) THF, 3 h

With 1H-imidazole; camphor-10-sulfonic acid; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; In acetone;

Reference yield:

: 127000-09-3
benzyl α-D-fucopyranoside

: 150650-42-3
phenylmethyl 6-deoxy-3,4-O-(1-methylidene)-2-O-(phenylmethyl)-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / TsOH / acetone / 1 h / 25 °C

2: 1.) NaH, imidazole, 2.) n-Bu₄NI / 1.) THF, from 0 to 25 deg C, 50 min, 2.) THF, 3 h

With 1H-imidazole; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; In acetone;

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 150650-42-3
phenylmethyl 6-deoxy-3,4-O-(1-methylidene)-2-O-(phenylmethyl)-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / CSA

2: 84 percent / TsOH / acetone / 1 h / 25 °C

3: 1.) NaH, imidazole, 2.) n-Bu₄NI / 1.) THF, from 0 to 25 deg C, 50 min, 2.) THF, 3 h

With 1H-imidazole; camphor-10-sulfonic acid; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; In acetone;